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Time Resolved Measurements of Soot Concentrations and Mean Particle Sizes during EUDC and ECE Cycles
(2002)
A system for the on-line/in-line measurement of soot particle sizes and concentrations in the undiluted exhaust gas of diesel engines was developed and successfully tested. The unit uses the individual attenuations of three different laser wavelengths and is combined with an optical cell (white principle) with adjustable path lengths from 2.5 to 15 meters.
The importance of obtaining simultaneous particle size and concentration values has grown up with continuing discussion of the health effects, of internal combustion engine generated particulate emissions and in particular of Diesel soot emissions. In the present work an aerosol measurement system is described that delivers information about particle size and concentration directly from the undiluted exhaust gas.
Using three laser diodes of different wavelengths which form one parallel light beam, each spectral attenuation is analysed by a single detector and the particle diameter and concentration is evaluated by the use of the Mie theory and shown on-line at a frequency of 1 Hz. The system includes an optical long-path-cell (White principle) with an adjustable path length from 2.5 to 15 m, which allows the analysis within a broad concentration range.
On-line measurements of the particulate emissions in the hot, undiluted exhaust of Diesel engines are presented under stationary and transient engine’s load conditions. Mean particle diameters well below 100 nm are detected for modern Diesel engines. The measured particle concentration corresponds excellently with the traditional gravimetrical measurements of the diluted exhaust. Additionally, measurements of particle emissions (mostly condensed hydricarbons) from a two-stroke engine are presented and discussed.
A prototype multiwavelength sensor able to characterise soot emissions in Diesel exhaust in terms of size and concentration has been tested against other methods for diesel particle measurements like electrical mobility sizing (SMPS) and raw exhaust gravimetric sampling (RES). Measurements carried out with the prototype sensor were correlated with the SMPS by assuming spherical and/or fractal aggregate morphology of the particles. Correlation of RES gravimetric data against the sensor and the SMPS led to the calculation of the solid density for soot particles to be 2.3 gr/cm3.
The flow field-flow fractionation (FIFFF) technique is a promising method for separating and analysing particles and large size macromolecules from a few nanometers to approximately 50 μm. A new fractionation channel is described featuring well defined flow conditions even for low channel heights with convenient assembling and operations features. The application of the new flow field-flow fractionation channel is proved by the analysis of pigments and other small particles of technical interest in the submicrometer range. The experimental results including multimodal size distributions are presented and discussed.
Zur Messung geringer Massenkonzentrationen und der Partikelgrößenverteilung unter hohen Druck- und Temperaturbedingungen, wie sie z.B. bei Überwachung des Gasstromes in Druckwirbelschichtfeuerungen oder in Druckkohlestaubfeuerungen vorkommen, wird ein kompensiertes Streulichtfotometer vorgeschlagen. Streulicht- und Transmissionswerte des Partikelkollektivs werden erfasst und miteinander verknüpft. Als Vorteil dieses Mess- und Auswerteprinzips ergibt sich im Gegensatz zu konventionellen Fotometern eine weitgehende Unempfindlichkeit gegenüber Fenster-Verschmutzung und Alterung von Komponenten. Das neue Konzept ist bis etwa 900 ºC einsatzfähig.