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In contrast to their traditional, non-interactive counterparts, interactive dynamic visualisations allow users to adapt their form and content to their individual cognitive skills and needs. Provided that the interactive features allow for intuitive use without increasing cognitive load, interactive videos should therefore lead to more efficient forms of learning. This notion was tested in an experimental study, where participants learned to tie four nautical knots of different complexity by watching either non-interactive or interactive videos. The results show that in the interactive condition, participants used the interactive features like stopping, replaying, reversing or changing speed to adapt the pace of the video demonstration. This led to an uneven distribution of their attention and cognitive resources across the videos, which was more pronounced for the difficult knots. Consequently users of non-interactive video presentations, needed substantially more time than users of the interactive videos to acquire the necessary skills for tying the knots.
Diode-array planar chromatography is a versatile tool for identification of pharmaceutical substances In this paper thirty-three compounds with benzodiazepine properties were investigated and the separating conditions for silica gel HPTLC plates and three mobile phases were optimized. Diode-array HPTLC makes it possible to identify all the compounds with high certainty down to a level of 20 ng. An algorithm for spectral recognition which is combined with R F values from the three separation steps into one fit factor is presented. This set of data is unique for each of the compounds investigated and enables unequivocal identification. The method is rapid, inexpensive, and sensitive down to a level of 20 ng mL −1.
Specific prototypes of sedimentation field flow fractionation devices (SdFFF) have been developed with relative success for cell sorting. However, no data are available to compare these apparatus with commercial ones. In order to compare with other devices mainly used for non-biological species, biocompatible systems were used for standard particle (latex: 3–10 μm of different size dispersities) separation development. In order to enhance size dependent separations, channels of reduced thickness were used (80 and 100 μm) and channel/carrier-phase equilibration procedures were necessary. For sample injection, the use of inlet tubing linked to the FFF accumulation wall, common for cell sorting, can be extended to latex species when they are eluted in the Steric Hyperlayer elution mode. It avoids any primary relaxation steps (stop flow injection procedure) simplifying series of elution processing. Mixtures composed of four different monodispersed latex beads can be eluted in 6 min with 100 μm channel thickness.
The three wavelength extinction method (3-WEM) was applied for the on-line particle analysisof suspensions of monodisperse latex beads and polydisperse metal oxide particles of industrialinterest. Comparative measurements were performed by photon correlation spectroscopy (PCS). Thedata of latex particles obtained by 3-WEM and PCS are in good agreement with the manufacture’svalues. Also, the values of oxide particles measured by means of the two techniques are in reasonableagreement despite of the irregular particle shape.Discrepancies are observed by comparing the oxideparticle size results with those of scanning electron microscopy, which is due to the broad sampledistributions and shape irregularities.
In thin-layer chromatography the development step distributes the sample throughout the layer, a process which strongly affects the reflection signals. The essential requirement for quantitative thinlayer chromatography is not a constant sample concentration but constant sample distribution in each sample spot. This makes evaporation of the mobile phase extremely important, because all tracks of a TLC plate must be dried uniformly. This paper shows that quantitative TLC is possible even if the concentration of the sample is not constant throughout the layer or if the distribution of the sample is not known. With uniform sample distribution, classical Kubelka-Munk theory is valid for isotropic scattering only. In the absence of this constraint classical Kubelka-Munk theory must be extended to situations where scattering is asymmetric. This can be achieved by modification of the original Kubelka-Munk equation. Extended theory is presented which is not only capable of describing asymmetrical scattering in TLC layers but also includes a formula for absorption and fluorescence in diode-array TLC. With this new theory all different formulas for diode-array thin-layer chromatographic evaluation are combined in one expression.
This paper focuses on the effects of differential mode delay (DMD) on the bandwidth of multimode optical fibres. First an analytical solution for the computation of the differential mode time delay is presented. The electrical field of each mode is calculated by the numerical solution of the Helmholtz equation. Based on this solution the modal power distribution as well as the fibre's impulse response under different launching conditions can be obtained.
Next, the refractive-index profile of two fibres is modelled on the basis of DMD measurements. It is shown that these measurements provide enough information to predict the fibre's propagation characteristics under different launch conditions (excitation conditions).
An interlaboratory comparison was carried out to evaluate the effectiveness of a method based on HPTLC in which reagent-free derivatization is followed by UV/fluorescence detection. The method was tested for the determination of sucralose (C12H19C13O8; (2R,3R,4R,5S,6R)-2-[(2R,3S,4S,5S)-2,5-bis(chloromethyl)-3,4-dihydroxyoxolan-2-yl]oxy-5-chloro-6-hydroxymethyl)oxane-3, 4-diol; CAS Registry No. 56038-13-2) in carbonated and still beverages at the proposed European regulatory limits. For still beverages, a portion of the sample was diluted with methanol-water. For carbonated beverages, a portion of the sample was degassed in an ultrasonic bath before dilution. Turbid beverages were filtered after dilution through an HPLC syringe filter. The separation of sucralose was performed by direct application on amino-bonded (NH2) silica gel HPTLC plates (no cleanup needed) with the mobile phase acetonitrile-water. Sucralose was determined after reagent-free derivatization at 190 degrees C; it was quantified by measurements of both UV absorption and fluorescence. The samples, both spiked and containing sucralose, were sent to 14 laboratories in five different countries. Test portions of a sample found to contain no sucralose were spiked at levels of 30.5, 100.7, and 299 mg/L. Recoveries ranged from 104.3 to 124.6% and averaged 112% for determination by UV detection; recoveries ranged from 98.4 to 101.3% and averaged 99.9% for determination by fluorescence detection. On the basis of the results for spiked samples (blind duplicates at three levels), as well as sucralose-containing samples (blind duplicates at three levels and one split level), the values for the RSDr ranged from 10.3 to 31.4% for determinations by UV detection and from 8.9 to 15.9% for determinations by fluorescence detection. The values for the RSDR values ranged from 13.5 to 31.4% for determinations by UV detection and from 8.9 to 20.7% for determinations by fluorescence detection.
Geothermal Energy in Germany
(2009)
Rotation of an elastic medium gives rise to a shift of frequency of its acoustic modes, i.e., the time-period vibrations that exist in it. This frequency shift is investigated by applying perturbation theory in the regime of small ratios of the rotation velocity and the frequency of the acoustic mode. In an expansion of the relative frequency shift in powers of this ratio, upper bounds are derived for the first-order and the second-order terms. The derivation of the theoretical upper bounds of the first-order term is presented for linear vibration modes as well as for stable nonlinear vibrations with periodic time dependence that can be represented by a Fourier series.
Silicon edges as one-dimensional waveguides for dispersion-free and supersonic leaky wedge waves
(2012)
Acoustic waves guided by the cleaved edge of a Si(111) crystal were studied using a laser-based angle-tunable transducer for selectively launching isolated wedge or surface modes. A supersonic leaky wedge wave and the fundamental wedge wave were observed experimentally and confirmed theoretically. Coupling of the supersonic wave to shear waves is discussed, and its leakage into the surface acoustic wave was observed directly. The velocity and penetration depth of the wedge waves were determined by contact-free optical probing. Thus, a detailed experimental and theoretical study of linear one-dimensional guided modes in silicon is presented.
The communication technologies for automatic me-ter reading (smart metering) and for energy production and distribution networks (smart grid) have the potential to be one of the first really highly scaled machine-to-machine-(M2M)-applications. During the last years two very promising devel-opments around the wireless part of smart grid communication were initialized, which possibly have an impact on the markets far beyond Europe and far beyond energy automation. Besides the specifications of the Open Metering System (OMS) Group, the German Federal Office for Information Security (Bundesamt für Sicherheit in der Informationstechnik, BSI) has designed a protection profile (PP) and a technical directive (TR) for the communication unit of an intelligent measurement sys-tem (smart meter gateway), which were released in March 2013. This design uses state-of-the-art technologies and prescribes their implementation in real-life systems. At first sight the expenditures for the prescribed solutions seem to be significant. But in the long run, this path is inevitable and comes with strategic advantages.
The energy supply of Offenburg University of Applied Sciences (HS OG) was changed from separate generation to trigeneration in 2007/2008. Trigeneration was installed for supplying heat, cooling and electrical power at HS OG. In this paper, trigeneration process and its modes of operation along with the layout of the energy facility at HS OG were described. Special emphasis was given to the operation schemes and control strategies of the operation modes: winter mode, transition mode and summer mode. The components used in the energy facility were also outlined. Monitoring and data analysis of the energy system was carried out after the commissioning of trigeneration in the period from 2008 to 2011. Thus, valuable performance data was obtained.
The design of control systems in large-scale CPV power plants will be more challenging in the future. Reasons are the increasing size of power plants, the requirements of grid operators, new functions, and new technological trends in industrial automation or communication technology. Concepts and products from fixed-mounted PV can only partly be adopted since control systems for sun-tracking installations are considerable more complex due to the higher quantity of controllable entities. The objective of this paper is to deliver design considerations for next generation control systems. Therefore, the work identifies new applications of future control systems categorized into operation, monitoring and maintenance domains. The key-requirements of the technical system and the application layer are identified. In the resulting section, new strategies such as a more decentralized architecture are proposed and design criteria are derived. The contribution of this paper should allow manufacturers and research institutes to consider the design criteria in current development and to place further research on new functions and control strategies precisely.
Multi-agent systems are a subject of continuously increasing interest in applied technical sciences. Smart grids are one evolving field of application. Numerous smart grid projects with various interpretations of multi-agent systems as new control concept arose in the last decade. Although several theoretical definitions of the term ‘agent’ exist, there is a lack of practical understanding that might be improved by clearly distinguishing the agent technologies from other state-of-the-art control technologies. In this paper we clarify the differences between controllers, optimizers, learning systems, and agents. Further, we review most recent smart grid projects, and contrast their interpretations with our understanding of agents and multi-agent systems. We point out that multi-agent systems applied in the smart grid can add value when they are understood as fully distributed networks of control entities embedded in dynamic grid environments; able to operate in a cooperative manner and to automatically (re-)configure themselves.
Hybrid SPECT/US
(2014)
Formal Description of Inductive Air Interfaces Using Thévenin's Theorem and Numerical Analysis
(2014)
With the development of new integrated circuits to interface radio frequency identification protocols, inductive air interfaces have become more and more important. Near field communication is not only able to communicate, but also possible to transfer power wirelessly and to build up passive devices for logistical and medical applications. In this way, the power management on the transponder becomes more and more relevant. A designer has to optimize power consumption as well as energy harvesting from the magnetic field. This paper discusses a model with simple equations to improve transponder antenna matching. Furthermore, a new numerical analysis technique is presented to calculate the coupling factors, inductions, and magnetic fields of multiantenna systems.
Mice and rats make up 95% of all animals used in medical research and drug discovery and development. Monitoring of physiological functions such as ECG, blood pressure, and body temperature over the entire period of an experiment is often required. Restraining of the animals in order to obtain this data can cause great inconvenience. The use of telemetric systems solves this problem and provides more reliable results. However, these devices are mostly equipped with batteries, which limit the time of operation or they use passive power supplies, which affects the operating range. The semi-passive telemetric implant being presented is based on RFID technology and overcomes these obstacles. The device is inductively powered using the magnetic field of a common RFID reader device underneath the cage, but is also able to operate for several hours autonomously. Being independent from the battery capacity, it is possible to use the implant over a long period of time or to re-use the device several times in different animals, thus avoiding the disadvantages of existing systems and reducing the costs of purchase and refurbishment.
Using patent information for identification of new product features with high market potential
(2014)