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The increasing use of artificial intelligence (AI) technologies across application domains has prompted our society to pay closer attention to AI’s trustworthiness, fairness, interpretability, and accountability. In order to foster trust in AI, it is important to consider the potential of interactive visualization, and how such visualizations help build trust in AI systems. This manifesto discusses the relevance of interactive visualizations and makes the following four claims: i) trust is not a technical problem, ii) trust is dynamic, iii) visualization cannot address all aspects of trust, and iv) visualization is crucial for human agency in AI.
Passive hybridization refers to a parallel connection of photovoltaic and battery cells on the direct current level without any active controllers or inverters. We present the first study of a lithium-ion battery cell connected in parallel to a string of four or five serially-connected photovoltaic cells. Experimental investigations were performed using a modified commercial photovoltaic module and a lithium titanate battery pouch cell, representing an overall 41.7 W-peak (photovoltaic)/36.8 W-hour (battery) passive hybrid system. Systematic and detailed monitoring of this system over periods of several days with different load scenarios was carried out. A scaled dynamic synthetic load representing a typical profile of a single-family house was successfully supplied with 100 % self-sufficiency over a period of two days. The system shows dynamic, fully passive self-regulation without maximum power point tracking and without battery management system. The feasibility of a photovoltaic/lithium-ion battery passive hybrid system could therefore be demonstrated.
IoT-Plattformen stellen ein zentrales Element für die Vernetzung von physischen Objekten und die Bereitstellung deren Daten für digitale Zwillinge dar. Der Markt für solche Plattformen ist in den vergangenen Jahren stark gewachsen. Bei inzwischen über 600 Anbietern ist die Wahl der „richtigen“ Plattform für das eigene Unternehmen keine triviale Aufgabe mehr. Dieser Beitrag soll Unternehmen im Auswahlprozess unterstützen, indem gängige Funktionen von IoT-Plattformen und Kriterien für die Auswahl von IoT-Plattformen aufgezeigt werden.
Wood juice, a liquid produced during wood processing, is a harmful waste that requires utilization. To achieve a circular economy, biowastes should be recycled, reducing fossil carbon usage. Therefore, the objective of this work was to examine the potential of wood juice as a feedstock for bioplastic synthesis by Bacillus sp. G8_19. Polyhydroxyalkanoate (PHA) syntheses using wood juice from Douglas fir trees and that from a mixture of spruce/fir trees were compared. It was found that the PHA content was higher after using wood juice from spruce/fir trees than that from Douglas fir trees (18.0% vs 6.1% of cell dry mass). Gas chromatography analysis showed that, with both wood juices, Bacillus sp. G8_19 accumulated poly(3-hydroxybutyrate-co-3-hydroxyvalerate). The content of 3-hydroxyvalerate (3HV) monomers was higher when spruce/fir wood juice was used (10.7% vs 1.9%). The C/N ratio did not have a statistically significant effect on the copolymer content in biomass, but it did significantly influence the 3HV content. The proposed concept may serve as an approach to wood waste valorization via production of biodegradable materials.
Interpreting seismic data requires the characterization of a number of key elements such as the position of faults and main reflections, presence of structural bodies, and clustering of areas exhibiting a similar amplitude versus angle response. Manual interpretation of geophysical data is often a difficult and time-consuming task, complicated by lack of resolution and presence of noise. In recent years, approaches based on convolutional neural networks have shown remarkable results in automating certain interpretative tasks. However, these state-of-the-art systems usually need to be trained in a supervised manner, and they suffer from a generalization problem. Hence, it is highly challenging to train a model that can yield accurate results on new real data obtained with different acquisition, processing, and geology than the data used for training. In this work, we introduce a novel method that combines generative neural networks with a segmentation task in order to decrease the gap between annotated training data and uninterpreted target data. We validate our approach on two applications: the detection of diffraction events and the picking of faults. We show that when transitioning from synthetic training data to real validation data, our workflow yields superior results compared to its counterpart without the generative network.
Properties of higher-order surface acoustic wave modes in Al(1-x)Sc(x)N / sapphire structures
(2021)
In this work, surface acoustic wave (SAW) modes and their dependence on propagation directions in epitaxial Al0.68Sc0.32N(0001) films on Al2O3(0001) substrates were studied using numerical and experimental methods. In order to find optimal propagation directions for higher-order SAW modes, phase velocity dispersion branches of Al0.68Sc0.32N on Al2O3 with Pt mass loading were computed for the propagation directions <11-20> and <1-100> with respect to the substrate. Experimental investigations of phase velocities and electromechanical coupling were performed for comparison with the numerical results. Simulations carried out with the finite element method (FEM) and with a Green function approach allowed identification of each wave type, including Rayleigh, Sezawa and shear horizontal wave modes. For the propagation direction <1-100>, significantly increased wave guidance of the Sezawa mode compared to other directions was observed, resulting in enhanced electromechanical coupling (k2eff = 1.6 %) and phase velocity (vphase = 6 km/s). We demonstrated, that selecting wave propagation in <1-100> with high mass density electrodes results in increased electromechanical coupling without significant reduction in phase velocities for the Sezawa wave mode. An improved combination of metallization, Sc concentration x, and SAW propagation direction is suggested which exhibits both high electromechanical coupling (k2eff > 6 %) and high velocity (vphase = 5.5 km/s) for the Sezawa mode.
In the present paper, the influence of locally varying microstructures in case of an AlSi12 cast aluminium alloy is investigated by means of extracting the test pieces from different removal positions and low cycle fatigue tests. The temperature-dependent damage mechanisms, the material specific defect types, sizes and their influence on the fatigue properties of two AlSi7 and AlSi12 cast aluminium alloys are studied. An extreme value statistics methodology is applied to predict maximum defect sizes expected in a critical surface volume from two-dimensional metallographic micrographs. A damage map for the AlSi12 cast aluminium alloy is presented explaining the influence of the temperature- and load-dependent damage mechanisms on the observed isothermal and thermomechanical lifetime behavior.
Detailed material investigations of the fatigue behavior of two cast aluminium alloys used in combustion engines are presented. The network of intermetallic phases of both aluminium alloys is characterized by means of detailed energy dispersive X-ray spectroscopy. In order to investigate the temperature-dependent fatigue behavior of the materials, tensile, low cycle and thermomechanical fatigue tests are performed over a wide temperature and loading range. The influence of the temperature dependence on the experimental results is discussed.
In this work, the influence of superimposed high cycle fatigue on the LCF/HCF and TMF/HCF lifetime is investigated for two cast aluminium alloys of the types AlSi7 and AlSi12. The replica technique is used to examine the short crack growth behavior under pure LCF and LCF/HCF loading. The observed short crack growth evolution explains the observed lifetime reduction with increasing HCF amplitudes.
Die Rolle des Aufsichtsrats wird zunehmend als eine strategische charakterisiert, ohne dies jedoch näher zu erläutern. Die aktuelle Diskussion zeigt, dass daraus Unschärfen in der Abgrenzung zur Rolle des Vorstands resultieren. In dem Beitrag wird die Rolle des Aufsichtsrats im Rahmen strategischer Entscheidungen präzisiert.
The aim of this review was to determine whether smartphone applications are reliable and valid to measure range of motion (RoM) in lower extremity joints. A literature search was performed up to October 2020 in the databases PubMed and Cochrane Library. Studies that reported reliability or validity of smartphone applications for RoM measurements were included. The study quality was assessed with the QUADAS-2 tool and baseline information, validity and reliability were extracted. Twenty-five studies were included in the review. Eighteen studies examined knee RoM, whereof two apps were analysed as having good to excellent reliability and validity for knee flexion (“DrGoniometer”, “Angle”) and one app showed good results for knee extension (“DrGoniometer”). Eight studies analysed ankle RoM. One of these apps showed good intra-rater reliability and excellent validity for dorsiflexion RoM (“iHandy level”), another app showed excellent reliability and moderate validity for plantarflexion RoM (“Coach’s Eye”). All other apps concerning lower extremity RoM had either insufficient results, lacked study quality or were no longer available. Some apps are reliable and valid to measure RoM in the knee and ankle joint. No app can be recommended for hip RoM measurement without restrictions.
A versatile liquid metal (LM) printing process enabling the fabrication of various fully printed devices such as intra- and interconnect wires, resistors, diodes, transistors, and basic circuit elements such as inverters which are process compatible with other digital printing and thin film structuring methods for integration is presented. For this, a glass capillary-based direct-write method for printing LMs such as eutectic gallium alloys, exploring the potential for fully printed LM-enabled devices is demonstrated. Examples for successful device fabrication include resistors, p–n diodes, and field effect transistors. The device functionality and easiness of one integrated fabrication flow shows that the potential of LM printing is far exceeding the use of interconnecting conventional electronic devices in printed electronics.
Significant progress in the development and commercialization of electrically conductive adhesives has been made. This makes shingling a very attractive approach for solar cell interconnection. In this study, we investigate the shading tolerance of two types of solar modules based on shingle interconnection: first, the already commercialized string approach, and second, the matrix technology where solar cells are intrinsically interconnected in parallel and in series. An experimentally validated LTspice model predicts major advantages for the power output of the matrix layout under partial shading. Diagonal as well as random shading of a 1.6-m2 solar module is examined. Power gains of up to 73.8 % for diagonal shading and up to 96.5 % for random shading are found for the matrix technology compared to the standard string approach. The key factor is an increased current extraction due to lateral current flows. Especially under minor shading, the matrix technology benefits from an increased fill factor as well. Under diagonal shading, we find the probability of parts of the matrix module being bypassed to be reduced by 40 % in comparison to the string module. In consequence, the overall risk of hotspot occurrence in matrix modules is decreased significantly.
The work focuses on predictive capabilities of fundamental cyclic plasticity and fatigue life models, which can be calibrated using limited amount of experiments as specific ones needed for more advanced models are often absent. The analyses are conducted for the synthetic case of exhaust manifold made from cast iron. The thermal boundary conditions from the forced convection were obtained from the computational fluid dynamics considered as a conjugate heat transfer problem. Two rate-independent and temperature-dependent material models were calibrated for structural analyses. Both were validated with experiments on isothermal and anisothermal levels. Sequential thermal–mechanical finite element simulations were performed. Two fatigue life models were employed. The first was a temperature-dependent strain-based fatigue life criterion calibrated from uniaxial data. The second was a temperature-independent energy-based fatigue life criterion resulting in twice lower life than the strain-based criterion, while none of the plasticity models made a significant difference in that prediction.
Cyclic micro-bending tests on fcc single crystal Ni-base Alloy 718 cantilevers with different crystal orientations were performed to analyze the influence of activated slip systems on dislocation plasticity, latent hardening and the Bauschinger effect. The investigations indicate that plasticity in single crystal micro-cantilevers is significantly influenced by two phenomena - dislocation interaction and dislocation pile-up at the neutral plane. Both phenomena occur at the same time. Their ratio seems to be determined by the activated slip systems. Slip trace analysis indicates that the activation of only one slip system leads to a strong localization of plasticity to a limited number of parallel slip bands. This results in low dislocation interaction and consequently pronounced pile-ups at the neutral plane. In multi slip orientation, the second slip system leads to activation of significantly more dislocation sources, causing a much earlier and more homogeneous elastic-plastic transition zone. In stress-strain hysteresis loops during bending, pronounced dislocation interaction in multi slip orientation leads to a more pronounced latent hardening. The results suggest that on a microstructural length scale, plasticity behavior is strongly affected by activated slip systems, which determine local dislocation phenomena. Based on the results presented in this paper, a finite element analysis of latent hardening and the Bauschinger effect using a single crystal plasticity model with latent kinematic hardening is presented in Part II.
Due to higher combustion chamber temperatures and pressures in efficient combustion engines, both the high-cycle and thermomechanical fatigue loads on service life-critical components, such as the cylinder head, are increasing. Material comparisons and analysis of damage behavior are very expensive and time-consuming using component tests. This study therefore develops a test method for cylinder head materials that takes into account the combined loading conditions from the above-mentioned loads and allows realistic temperature transients and gradients on near-component samples. The near-component cylinder head sample represents the failure-critical exhaust valve crosspiece and is tested in a test rig specially designed with the aid of conjugate heat transfer simulations. In the test rig, the sample is subjected to thermal stress by a hot gas burner and to mechanical stress by a high-frequency pulsator. Optical crack detection allows permanent observation of fatigue crack growth and crack closure during the test. Fractographic and metallo-graphic examinations of the fracture areas as well as analyses of the damage patterns show that loads close to engine operation can be set in this way and their influences on the damage can be monitored.
Quantifying the midsole material characteristics of athletic footwear is a standard task in footwear research and development. Current material testing protocols primarily focus on the determination of cushioning properties of the heel region or the quantification of the midsole properties as one assembly. However, midsoles possess different spatial material properties that have not been quantified from previous methodologies. Therefore, new material testing methods are required to quantify the local material response of athletic footwear. We developed a cyclical force-controlled material testing protocol for the determination of non-homogeneously distributed material stiffness with a high spatial resolution. In five prototype shoes varying in their stiffness distribution, we found that the material properties can be reliably measured across the midsole. Furthermore, we observed a characteristic non-linear material response regardless of the midsole location. We found that the material stiffness increased with an increase of the applied force and that this effect is further intensified by higher testing cycles. Additionally, the obtained midsole stiffness depends on the geometry of the midsole. We explored different approaches to reduce the measurement time of the testing protocol and found that the number of measurements can be reduced by 70% using 2 D-interpolation procedures. Determining the spatial material properties of midsoles needs to be considered to understand foot-shoe interactions. Furthermore, this measurement protocol can be used for quality control within the footwear and can be adapted for considering the effects of different running styles or speeds on ground force application characteristics.
Die vorliegende Arbeit gibt einen Überblick über das Verhältnis zwischen Nutzen und Einschränkungen eines frühneuzeitlichen Riefelharnisches auf die Biomechanik des Menschen. Zu den zentralen Ergebnissen gehört, dass die Rüstung eine gewisse Einschränkung der Beweglichkeit bringt, jedoch durch verschiedene mechanische Konzepte versucht wurde, diese größtmöglich zu minimieren. Besonders das sogenannte Geschübe stellt hierbei einen Kompromiss zwischen Beweglichkeit und Schutzfunktion dar und findet vor allem im Bereich der Gelenke Anwendung. Steife Strukturen werden an Stellen eingesetzt, die kaum Bewegungsfreiheit fordern. Zu diesen Bereichen gehören beispielsweise der Brustkorb oder obere Teile des Rückens. Der Vorteil der steiferen Teile der Rüstung ist ihre erhöhte Schutzfunktion, die ein geringeres Verletzungsrisiko mit sich bringt.
Uphill training is applied to induce specific overload on the musculoskeletal system to improve sprinting mechanics. This study aimed to identify unique kinematic features of uphill sprinting at different slopes and to suggest practical implications based on comparisons we early stance phase. At take-off, steeper slopes induced significantly more extended joint angles and higher ROMs during the late stance phase. Compared with moderate slopes, more anti-phase coordination patterns were detected at steeper slopes. Thus, uphill sprinting at steeper slopes shares essential kinematic features with the early acceleration phase of level sprinting. Moderate inclinations induce biomechanical adaptations similar to those in the late acceleration phase of level sprinting. Hence, the specific transfer of uphill sprinting to acceleration depends on the slope inclinations.
Fünf Jahre vor seinem Tod, im Jahr 1932, wurde der berühmte französische Komponist Maurice Ravel (1875–1937), der an einer frontotemporalen Demenz (M. Pick) mit primär progressiver Aphasie litt, bei einem Unfall verletzt, als er in einem Pariser Taxi saß. In diesem Fallbericht wird der Unfallmechanismus unter bestimmten Annahmen dargestellt und diskutiert. Ausgehend von diesen Überlegungen ist ein Unfall bei geringer Kollisionsgeschwindigkeit wahrscheinlich. Trotz eines Unfalls mit nur geringer Geschwindigkeit ist nicht von der Hand zu weisen, dass dieser Unfall zumindest zu einer deutlichen Verschlimmerung der Krankheitssymptome geführt haben könnte, da Ravel seit diesem Taxiunfall bis zu seinem Tod keine weiteren Kompositionen mehr vollendet hat.
In dieser Arbeit wird ein historischer Fallbericht des bis heute weit über seine Landesgrenzen bekannten italienischen Kriminalanthropologen Cesare Lombroso (1835–1909) vorgestellt. In diesem Fallbericht wird der berüchtigte und psychisch auffällige Dieb Pietro Bersone mit Hilfe eines sog. Hydrosphygmographen überführt, einem zur damaligen Zeit neuartigen technischen Gerät, das den Puls nicht-invasiv aufzeichnen konnte. Lombroso ist vermutlich einer der ersten, wenn nicht sogar der erste, der durch den Einsatz eines solchen Geräts die Idee zum „Lügendetektor“ vorweggenommen hat. Die vorgestellte Textstelle aus Lombrosos Buch „Neue Fortschritte in den Verbrecherstudien“ ist daher ein besonderes Fundstück auch für die Geschichte der Polygraphie.
Surface acoustic waves are propagated toward the edge of an anisotropic elastic medium (a silicon crystal), which supports leaky waves with a high degree of localization at the tip of the edge. At an angle of incidence corresponding to phase matching with this leaky wedge wave, a sharp peak in the reflection coefficient of the surface wave was found. This anomalous reflection is associated with efficient excitation of the leaky wedge wave. In laser ultrasound experiments, surface acoustic wave pulses were excited and their reflection from the edge of the sample and their partial conversion into leaky wedge wave pulses was observed by optical probe-beam deflection. The reflection scenario and the pulse shapes of the surface and wedge-localized guided waves, including the evolution of the acoustic pulse traveling along the edge, have been confirmed in detail by numerical simulations.
Propagation of acoustic waves is considered in a system consisting of two stiff quarter-spaces connected by a planar soft layer. The two quarter-spaces and the layer form a half-space with a planar surface. In a numerical study, surface waves have been found and analyzed in this system with displacements that are localized not only at the surface, but also in the soft layer. In addition to the semi-analytical finite element method, an alternative approach based on an expansion of the displacement field in a double series of Laguerre functions and Legendre polynomials has been applied.
It is shown that a number of branches of the mode spectrum can be interpreted and remarkably well described by perturbation theory, where the zero-order modes are the wedge waves guided at a rectangular edge of the stiff quarter-spaces or waves guided at the edge of a soft plate with rigid surfaces.
For elastic moduli and densities corresponding to the material combination PMMA–silicone–PMMA, at least one of the branches in the dispersion relation of surface waves trapped in the soft layer exhibits a zero-group velocity point.
Potential applications of these 1D guided surface waves in non-destructive evaluation are discussed.
Objective: To quantify the effect of inhaled 5% carbon-dioxide/95% oxygen on EEG recordings from patients in non-convulsive status epilepticus (NCSE).
Methods: Five children of mixed aetiology in NCSE were given high flow of inhaled carbogen (5% carbon dioxide/95% oxygen) using a face mask for maximum 120s. EEG was recorded concurrently in all patients. The effects of inhaled carbogen on patient EEG recordings were investigated using band-power, functional connectivity and graph theory measures. Carbogen effect was quantified by measuring effect size (Cohen's d) between "before", "during" and "after" carbogen delivery states.
Results: Carbogen's apparent effect on EEG band-power and network metrics across all patients for "before-during" and "before-after" inhalation comparisons was inconsistent across the five patients.
Conclusion: The changes in different measures suggest a potentially non-homogeneous effect of carbogen on the patients' EEG. Different aetiology and duration of the inhalation may underlie these non-homogeneous effects. Tuning the carbogen parameters (such as ratio between CO2 and O2, duration of inhalation) on a personalised basis may improve seizure suppression in future.
Time-Sensitive Networking (TSN) is the most promising time-deterministic wired communication approach for industrial applications. To extend TSN to "IEEE 802.11" wireless networks two challenging problems must be solved: synchronization and scheduling. This paper is focused on the first one. Even though a few solutions already meet the required synchronization accuracies, they are built on expensive hardware that is not suited for mass market products. While next Wi-Fi generation might support the required functionalities, this paper proposes a novel method that makes possible high-precision wireless synchronization using commercial low-cost components. With the proposed solution, a standard deviation of synchronization error of less than 500 ns can be achieved for many use cases and system loads on both CPU and network. This performance is comparable to modern wired real-time field busses, which makes the developed method a significant contribution for the extension of the TSN protocol to the wireless domain.
Digitale Lernszenarien in der Hochschullehre. Bedeutung und Funktion aus Sicht von Studierenden
(2021)
Bedingt durch die Coronapandemie wurde in den Informatikkursen Software Engineering und Computernetze an der Hochschule Offenburg ein Lernsetting entwickelt, das mehrere digitale Lernszenarien (Online-Sessions, Lernvideos, Wikis, Quiz, Foren und die selbst entwickelte Lernplattform MILearning) integriert. Im Wintersemester 2020/2021 fand eine Evaluierung statt, um den Einsatz der unterschiedlichen digitalen Lernszenarien in der aktuellen Situation zu bewerten und um zu entscheiden, welche Lernszenarien sinnvoll für einen Einsatz nach der Pandemie sind. Aus dem Blickwinkel des Didaktischen Designs spielen dabei die Eignung der Szenarien für die Wissensvermittlung, die Aktivierung der Studierenden und die Betreuung bei Fragen und Problemen eine wichtige Rolle. Die Ergebnisse zeigen, dass Studierende das Lernsetting intensiv nutzen und die angebotenen digitalen Lernszenarien lernförderlich kombinieren.
A Hybrid Optoelectronic Sensor Platform with an Integrated Solution‐Processed Organic Photodiode
(2021)
Hybrid systems, unifying printed electronics with silicon‐based technology, can be seen as a driving force for future sensor development. Especially interesting are sensing elements based on printed devices in combination with silicon‐based high‐performance electronics for data acquisition and communication. In this work, a hybrid system integrating a solution‐processed organic photodiode in a silicon‐based system environment, which enables flexible device measurement and application‐driven development, is presented. For performance evaluation of the integrated organic photodiode, the measurements are compared to a silicon‐based counterpart. Therefore, the steady state response of the hybrid system is presented. Promising application scenarios are described, where a solution‐processed organic photodiode is fully integrated in a silicon system.
In the last decade, deep learning models for condition monitoring of mechanical systems increasingly gained importance. Most of the previous works use data of the same domain (e.g., bearing type) or of a large amount of (labeled) samples. This approach is not valid for many real-world scenarios from industrial use-cases where only a small amount of data, often unlabeled, is available.
In this paper, we propose, evaluate, and compare a novel technique based on an intermediate domain, which creates a new representation of the features in the data and abstracts the defects of rotating elements such as bearings. The results based on an intermediate domain related to characteristic frequencies show an improved accuracy of up to 32 % on small labeled datasets compared to the current state-of-the-art in the time-frequency domain.
Furthermore, a Convolutional Neural Network (CNN) architecture is proposed for transfer learning. We also propose and evaluate a new approach for transfer learning, which we call Layered Maximum Mean Discrepancy (LMMD). This approach is based on the Maximum Mean Discrepancy (MMD) but extends it by considering the special characteristics of the proposed intermediate domain. The presented approach outperforms the traditional combination of Hilbert–Huang Transform (HHT) and S-Transform with MMD on all datasets for unsupervised as well as for semi-supervised learning. In most of our test cases, it also outperforms other state-of-the-art techniques.
This approach is capable of using different types of bearings in the source and target domain under a wide variation of the rotation speed.
It is important to minimize the unscheduled downtime of machines caused by outages of machine components in highly automated production lines. Considering machine tools such as, grinding machines, the bearing inside of spindles is one of the most critical components. In the last decade, research has increasingly focused on fault detection of bearings. In addition, the rise of machine learning concepts has also intensified interest in this area. However, up to date, there is no single one-fits-all solution for predictive maintenance of bearings. Most research so far has only looked at individual bearing types at a time.
This paper gives an overview of the most important approaches for bearing-fault analysis in grinding machines. There are two main parts of the analysis presented in this paper. The first part presents the classification of bearing faults, which includes the detection of unhealthy conditions, the position of the error (e.g. at the inner or at the outer ring of the bearing) and the severity, which detects the size of the fault. The second part presents the prediction of remaining useful life, which is important for estimating the productive use of a component before a potential failure, optimizing the replacement costs and minimizing downtime.
Mit zunehmender Datenverfügbarkeit wird der Einsatz Maschinellen Lernens zur Steuerung und Optimierung von Supply Chains attraktiver, da die Qualität der Datenauswertung erhöht und gleichzeitig der Aufwand gesenkt werden kann. Anhand des SCOR-Modells werden exemplarische Ansätze als Orientierungshilfe eingeordnet und dazu passende Verfahren des Maschinellen Lernens vorgestellt.
We present a video-densitometric high-performance thin-layer chromatography (HPTLC) quantification method for patulin in apple juice, developed in a vertical chamber from the starting point to a distance of 50 mm, using MTBE, n-pentane (9 + 5, v/v) as mobile phase. After separation the plate is sprayed with methyl-benzothiazolinone hydrazone hydrochloride monohydrate (MBTH) solution (40 mg in 20 mL methanol) and heated at 105 °C for 15 min. Patulin zones are transformed into yellow spots. The quantification is based on direct measurements using an inexpensive 48-bit flatbed scanner for color measurements (in red, green, and blue). Evaluation of the blue channel makes the measurements very specific. Quantification in fluorescence was also done by use of a 16-bit CCD-camera and UV-366 nm illumination as well as using a HPTLC DAD-scanner. For linearization the extended Kubelka–Munk expression for data transformation was used. The range of linearity covers more than two magnitudes and lies between 5 and 800 ng patulin. The extraction of 20 g apple juice and an extract application on plate up to 50 µL allows statistically defined checking the limit of detection (LOD) of 50 ng patulin per track, which is equivalent to 50 µg patulin per kg apple juice.
The compliant nature of distal limb muscle-tendon units is traditionally considered suboptimal in explosive movements when positive joint work is required. However, during accelerative running, ankle joint net mechanical work is positive. Therefore, this study aims to investigate how plantar flexor muscle-tendon behavior is modulated during fast accelerations. Eleven female sprinters performed maximum sprint accelerations from starting blocks, while gastrocnemius muscle fascicle lengths were estimated using ultrasonography. We combined motion analysis and ground reaction force measurements to assess lower limb joint kinematics and kinetics, and to estimate gastrocnemius muscle-tendon unit length during the first two acceleration steps. Outcome variables were resampled to the stance phase and averaged across three to five trials. Relevant scalars were extracted and analyzed using one-sample and two-sample t-tests, and vector trajectories were compared using statistical parametric mapping. We found that an uncoupling of muscle fascicle behavior from muscle-tendon unit behavior is effectively used to produce net positive mechanical work at the joint during maximum sprint acceleration. Muscle fascicles shortened throughout the first and second steps, while shortening occurred earlier during the first step, where negative joint work was lower compared with the second step. Elastic strain energy may be stored during dorsiflexion after touchdown since fascicles did not lengthen at the same time to dissipate energy. Thus, net positive work generation is accommodated by the reuse of elastic strain energy along with positive gastrocnemius fascicle work. Our results show a mechanism of how muscles with high in-series compliance can contribute to net positive joint work.
Despite increasing budgets for social media activities and a wide variety of performance measurement possibilities, many companies do not measure the performance of their social media activities. Research shows that those companies that measure the performance of social media activities use incorrect, too few or inappropriate metrics. A central problem is that there is often an inadequate performance measurement process. This article presents a process that focuses on the objectives of social media activities. In phase one of this process, suitable metrics are selected and target values are defined based on these objectives. In phase two, data are collected and analysed. Finally, actions are defined. The developed process helps companies to measure the performance of their social media activities.