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A systematic toxicological analysis procedure using high-performance thin layer chromatography in combination with fibre optical scanning densitometry for identification of drugs in biological samples is presented. Two examples illustrate the practicability of the technique. First, the identification of a multiple intake of analgesics: codeine, propyphenazone, tramadol, flupirtine and lidocaine, and second, the detection of the sedative diphenhydramine. In both cases, authentic urine specimens were used. The identifications were carried out by an automatic measurement and computer-based comparison of in situ UV spectra with data from a compiled library of reference spectra using the cross-correlation function. The technique allowed a parallel recording of chromatograms and in situ UV spectra in the range of 197–612 nm. Unlike the conventional densitometry, a dependency of UV spectra by concentration of substance in a range of 250–1000 ng/spot was not observed.
Process engineering focuses on the design, operation, control and optimization of chemical, physical and biological processes and has applications in many industries. Process Intensification is the key development approach in the modern process engineering. The proposed Advanced Innovation Design Approach (AIDA) combines the holistic innovation process with the systematic analytical and problem solving tools of the theory of inventive problem solving TRIZ. The present paper conceptualizes the AIDA application in the field of process engineering and especially in combination with the Process Intensification. It defines the AIDA innovation algorithm for process engineering and describes process mapping, problem ranking, and concept design techniques. The approach has been validated in several industrial case studies. The presented research work is a part of the European project “Intensified by Design® platform for the intensification of processes involving solids handling”.
The Advanced Innovation Design Approach is a holistic methodology for enhancing innovative and competitive capability of industrial companies. AIDA can be considered as an open mindset, an individually adaptable range of strongest innovation techniques such as comprehensive front-end innovation process, advanced innovation methods, best tools and methods of the TRIZ methodology, organizational measures for accelerating innovation, IT-solutions for Computer-Aided Innovation, and other innovation methods, elaborated in the recent decade in the industry and academia
Recent advances in spiked shoe design, characterized by increased longitudinal stiffness, thicker midsole foams, and reconfigured geometry are considered to improve sprint performance. However, so far there is no empirical data on the effects of advanced spikes technology on maximal sprinting speed (MSS) published yet. Consequently, we assessed MSS via ‘flying 30m’ sprints of 44 trained male (PR: 10.32 s - 12.08 s) and female (PR: 11.56 s - 14.18 s) athletes, wearing both traditional and advanced spikes in a randomized, repeated measures design. The results revealed a statistically significant increase in MSS by 1.21% on average when using advanced spikes technology. Notably, 87% of participants showed improved MSS with the use of advanced spikes. A cluster analysis unveiled that athletes with higher MSS may benefit to a greater extent. However, individual responses varied widely, suggesting the influence of multiple factors that need detailed exploration. Therefore, coaches and athletes are advised to interpret the promising performance enhancements cautiously and evaluate the appropriateness of the advanced spike technology for their athletes critically.
Membrane distillation (MD) is a thermal separation process which possesses a hydrophobic, microporous
membrane as vapor space. A high potential application for MD is the concentration of hypersaline brines, such as
e.g. reverse osmosis retentate or other saline effluents to be concentrated to a near saturation level with a Zero
Liquid Discharge process chain. In order to further commercialize MD for these target applications, adapted MD
module designs are required along with strategies for the mitigation of membrane wetting phenomena. This
work presents the experimental results of pilot operation with an adapted Air Gap Membrane Distillation
(AGMD) module for hypersaline brine concentration within a range of 0–240 g NaCl /kg solution. Key performance
indicators such as flux, GOR and thermal efficiency are analyzed. A new strategy for wetting mitigation
by active draining of the air gap channel by low pressure air blowing is tested and analyzed. Only small reductions
in flux and GOR of 1.2% and 4.1% respectively, are caused by air sparging into the air gap channel.
Wetting phenomena are significantly reduced by avoiding stagnant distillate in the air gap making the air blower
a seemingly worth- while additional system component.
Am 1. Juli 2022 trafen sich im Rahmen des Abschlusskolloquiums des Projekts ACA-Modes rund 60 Teilnehmende aus Forschung, Lehre und Industrie zu einer internationalen Konferenz an der Hochschule Offenburg. Hier wurden die Projektergebnisse rund um die erfolgreiche Implementierung modellprädiktiver Regelstrategien vorgestellt, aktuelle Fragestellungen diskutiert und Entwicklungspfade hin zu einem netzdienlichen Betrieb von Energieverbundsystemen skizziert.
Hintergrund
In diesem Artikel wird ein Überblick und Vergleich der am häufigsten verwendeten zementierten Hüftschäfte, gruppiert in die verschiedenen Schafttypen und Zementmanteldicken, gegeben, um zu sehen, welche Kombination gut abschneidet.
Methodik
Aus dem Endoprothesenregister Deutschland wurden die Revisionsraten zementierter Schaftarten kategorisiert und die Revisionsraten von 3 und 5 Jahren erfasst und analysiert. Für die Recherche lag die Konzentration auf den Schäften Exeter, C‑Stem, MS-30, Excia, Bicontact, Charnley, Müller Geradschaft, Twinsys, Corail, Avenir, Quadra und dem Lubinus SP II. Ein wichtiger Aspekt lag darin, welcher Schaft favorisiert implantiert wird und welche Zementiertechnik in Hinblick auf die geplante Zementmanteldicke angewendet wird. Um einen Trend in der zementierten Hüftendoprothetik herauszufinden, wurden zusätzlich die Daten des dänischen, schwedischen, norwegischen, schweizerischen, neuseeländischen, englischen und australischen Endoprothesenregister verglichen.
Ergebnisse und Schlussfolgerung
Die meisten Länder nutzen zementierte Prothesen nach dem Kraftschlussprinzip (Exeter, MS30, C‑Stem etc.) oder dem Formschlussprinzip (Charnley, Excia, Bicontact), welche mit einer Zementmanteldicke von 2–4 mm implantiert werden. Jedoch hat sich in Deutschland und der Schweiz ein Trend zur Line-to-Line-Technik, mit einer geplanten Zementmanteldicke von 1 mm (Twinsys, Corail, Avenir, Quadra) aufgezeigt, dem Prinzip der Müller-Geradschaft-Prothese und der Kerboul-Charnley-Prothese folgend, auch wenn diese an sich als „french paradoxon“ postuliert werden. In den EPRD-5-Jahres-Ergebnissen scheinen die neueren Line-to-Line-Prothesen etwas schlechter abzuschneiden. Die besten Ergebnisse erzielt der „MS 30“ in Deutschland und der „Exeter“ in England. Hierbei handelt es sich um polierte Geradschäfte mit Zentraliser und Subsidence-Raum an der Spitze mit einem 2–4 mm Zementmantel in guter Zementiertechnik.
Alexander von Humboldt, a German scientist and explorer of the 19th century, viewed the natural world holistically and described the harmony of nature among the diversity of the physical world as a conjoining between all physical disciplines. He noted in his diary: “Everything is interconnectedness.”
The main feature of Humboldt’s pioneering work was later named “Humboldtian science”, meaning the accurate study of interconnected real phenomena in order to find a definite law and a dynamic cause.
Following Humboldt's idea of nature, an Internet edition of his works must preserve the author’s original intention, retain an awareness of all relevant works, and still adhere to the requirements of scholarly edition.
At the present time, however, the highly unconventional form of his publications has undermined the awareness and a comprehensive study of Humboldt’s works.
Digital libraries should supply dynamic links to sources, maps, images, graphs and relevant texts. New forms of interaction and synthesis between humanistic texts and scientific observation need to be created.
Information technology is the only way to do justice to the broad range of visions, descriptions and the idea of nature of Humboldt’s legacy. It finally leads to virtual research environments as an adequate concept to redesign our digital archives, not only for Humboldt’s documents, but for all interconnected data.
Running footwear is continuously being modified and improved; however, running-related overuse injury rates remain high. Nevertheless, novel manufacturing processes enable the production of individualized running shoes that can fit the individual needs of runners, with the potential to reduce injury risk. For this reason, it is essential to investigate functional groups of runners, a collective of runners who respond similarly to a footwear intervention. Therefore, the objective of this study was to develop a framework to identify functional groups based on their individual footwear response regarding injury-specific running-related risk factors for Achilles tendinopathy, Tibial stress fractures, Medial tibial stress syndrome, and Patellofemoral pain syndrome. In this work, we quantified the footwear response patterns of 73 female and male participants when running in three different footwear conditions using unsupervised learning (k-means clustering). For each functional group, we identified the footwear conditions minimizing the injury-specific risk factors. We described differences in the functional groups regarding their running style, anthropometric, footwear perception, and demographics. The results implied that most functional groups showed a tendency for a single footwear condition to reduce most biomechanical risk factors for a specific overuse injury. Functional groups often differed in their hip and pelvis kinematics as well as their subjective rating of the footwear conditions. The footwear intervention only partially affected biomechanical risk factors attributed to more proximal joints. Due to its adaptive nature, the framework could be applied to other footwear interventions or performance-related biomechanical variables.
The authors present an abiotically catalyzed glucose fuel cell and demonstrate its application as energy harvesting power source for a cardiac pacemaker. This is enabled by an optimized DC-DC converter operating at 40 % conversion efficiency, which surpasses commercial low-power DC-DC converters. The required fuel cell surface area can thus be reduced from about 125 cm2 to 18 cm2, which would allow for its direct integration onto the pacemaker casing.
An Extraction Method for 17α-Ethinylestradiol from Water using a new kind of monolithic Stir-bar
(2015)
We present a video-densitometric high-performance thin-layer chromatography (HPTLC) quantification method for patulin in apple juice, developed in a vertical chamber from the starting point to a distance of 50 mm, using MTBE, n-pentane (9 + 5, v/v) as mobile phase. After separation the plate is sprayed with methyl-benzothiazolinone hydrazone hydrochloride monohydrate (MBTH) solution (40 mg in 20 mL methanol) and heated at 105 °C for 15 min. Patulin zones are transformed into yellow spots. The quantification is based on direct measurements using an inexpensive 48-bit flatbed scanner for color measurements (in red, green, and blue). Evaluation of the blue channel makes the measurements very specific. Quantification in fluorescence was also done by use of a 16-bit CCD-camera and UV-366 nm illumination as well as using a HPTLC DAD-scanner. For linearization the extended Kubelka–Munk expression for data transformation was used. The range of linearity covers more than two magnitudes and lies between 5 and 800 ng patulin. The extraction of 20 g apple juice and an extract application on plate up to 50 µL allows statistically defined checking the limit of detection (LOD) of 50 ng patulin per track, which is equivalent to 50 µg patulin per kg apple juice.
An isomorphous series of 10 microporous copper-based metal–organic frameworks (MOFs) with the general formulas ∞3[{Cu3(μ3-OH)(X)}4{Cu2(H2O)2}3(H-R-trz-ia)12] (R = H, CH3, Ph; X2– = SO42–, SeO42–, 2 NO32– (1–8)) and ∞3[{Cu3(μ3-OH)(X)}8{Cu2(H2O)2}6(H-3py-trz-ia)24Cu6]X3 (R = 3py; X2– = SO42–, SeO42– (9, 10)) is presented together with the closely related compounds ∞3[Cu6(μ4-O)(μ3-OH)2(H-Metrz-ia)4][Cu(H2O)6](NO3)2·10H2O (11) and ∞3[Cu2(H-3py-trz-ia)2(H2O)3] (12Cu), which are obtained under similar reaction conditions. The porosity of the series of cubic MOFs with twf-d topology reaches up to 66%. While the diameters of the spherical pores remain unaffected, adsorption measurements show that the pore volume can be fine-tuned by the substituents of the triazolyl isophthalate ligand and choice of the respective copper salt, that is, copper sulfate, selenate, or nitrate.
Objective: This paper deals with the design and the optimization of mechatronic devices.
Introduction: Comparing with existing works, the design approach presented in this paper aims to integrate optimization in the design phase of complex mechatronic systems in order to increase the efficiency of this method.
Methods: To solve this problem, a novel mechatronic system design approach has been developed in order to take the multidisciplinary aspect and to consider optimization as a tool that can be used within the embodiment design process to build mechatronic solutions from a set of solution concepts designed with innovative or routine design methods.
Conclusions: This approach has then been applied to the design and optimization of a wind turbine system that can be implemented to autonomously supply a mountain cottage.
Ein tiefgreifendes Verständnis des zyklischen Plastizitätsverhaltens metallischer Werkstoffe ist sowohl für die Optimierung der Materialeigenschaften als auch für die industrielle Auslegung und Fertigung von Bauteilen von hoher Relevanz. Insbesondere moderne Legierungen wie Duplex-Stähle zeigen unter Lastumkehr aufgrund des komplexen mehrphasigen Gefüges sowie der Neigung zu verschiedenen Ausscheidungsreaktionen einen ausgeprägten Bauschinger-Effekt, welcher bei technischen Umformvorgängen berücksichtigt werden muss. Der Bauschinger-Effekt begründet sich maßgeblich in der Entstehung von Rückspannungen, welche aus dem unterschiedlichen Plastizitätsverhalten der austenitischen und ferritischen Phase resultieren. Instrumentierte Mikroindenter-Versuche in ausgewählten Ferrit- und Austenitkörnern haben gezeigt, dass austenitische Gefügebestandteile durch einen deutlich früheren Fließbeginn sowie eine stärkere Rückplastifizierung während der Entlastung charakterisiert sind. Zudem wurde nachgewiesen, dass Ausscheidungen im Rahmen einer 475°C-Versprödung diesen Phasenunterschied verstärken und somit in einem höheren Bauschinger-Effekt resultieren.
Die Ziele des Projekts waren die Einführung der Zellseparations-Technik „Feldfluss-Fraktionierung“ (FFF) zur Analyse und Fraktionierung von Hefezellen zur Weinherstellung, sowie deren Weiterentwicklung und Optimierung für den Praxiseinsatz, insbesondere Auswahl einer einfachen FFF-Variante, Vereinfachung und Kostenoptimierung, um ein für Weinbaubetriebe erschwingliches FFF-Gerät anbieten zu können. Des Weiteren sollten FFF-Techniken als online Überwachung während des Wein-Fermentationsprozesses untersucht werden. Zur Qualitätsüberwachung war es wünschenswert unerwünschte Veränderungen während des Fermentationsprozesses frühzeitig erkennen zu können, um dann zur Qualitätsoptimierung gezielte Maßnahmen gegen unerwünschte Veränderungen vornehmen zu können. Das Projekt war auch dafür gedacht als Modell-Charakter bzw. als Pilotprojekt für andere auf dem Gärungswege durch Mikroorganismen hergestellte Produkte im Lebensmittel- oder biotechnologischen Bereich zu dienen.
Soot particles emitted from a light duty (LD) Volkswagen diesel engine running at different operating points (speed and torque levels) are analyzed for mean size determination using a laser‐based three Wavelength Extinction Method (3‐WEM). For this reason, collected soot samples are suspended using an appropriate sample preparation technique with optimized conditions of sonication as it revealed its effect on the soot mean particle size measured by 3‐WEM.
An online Scanning Mobility Particle Analyzer (SMPS) is also used to measure soot emission at identical engine operating points. Size values obtained from SMPS are lower than those of suspended soot samples obtained from 3‐WEM. The size discrepancies are mainly related to the required sample preparation procedure employed for 3‐WEM measurements. The engine operating points affect, differently, the size measurements obtained from SMPS and 3‐WEM.
Sedimentation Field‐Flow Fractionation (SdFFF) is used for density determination of soot samples based on size measurements of fractions collected at peak maxima of fractograms using the off‐line hyphenation with 3‐WEM. It is assumed that a size dependent separation of soot particles occurred with a uniform particle density over the whole size distribution. An average density value is used for the conversion of soot fractograms to size distributions. Discrepancies are also found with size distribution profiles obtained from SMPS for the same engine operating points, due to the sample preparation procedure employed for SdFFF measurements.
In der Planungs- und Betriebspraxis herrscht im Bereich der Betriebsführung von thermisch aktivierten Bauteilsystemen und insbesondere der thermisch trägen Bauteilaktivierung noch große Unsicherheit. Trotz einer weiten Verbreitung dieser Systeme im Neubau von Nichtwohngebäuden hat sich bis heute keine einheitliche Betriebsführungsstrategie durchgesetzt. Vielmehr kritisieren Bauherren und Nutzer regelmäßig zu hohe bzw. niedrige Raumtemperaturen in den Übergangsjahreszeiten und bei Wetterwechsel sowie generell eine mangelhafte Regelbarkeit. Demgegenüber weisen Monitoringprojekte immer wieder einen hohen thermischen Komfort in diesen Gebäuden nach. Offensichtlich unterscheiden sich hier subjektiv empfundene Behaglichkeit und objektiv gemessener Komfort. Gleichzeitig sind Heiz- und Kühlkonzepte mit Flächentemperierung dann besonders energieeffizient, wenn das Regelkonzept auf deren thermische Trägheit angepasst ist. Eine gute Regelung gewährleistet also einen hohen thermischen Komfort und sorgt für einen möglichst niedrigen Energieeinsatz. Das Rechenverfahren mit Anlagenaufwandszahlen (in Anlehnung an DIN V 18599) bietet eine gute Möglichkeit, Anlagenkonzepte inklusive deren Betriebsführungsstrategie zu bewerten. Damit ist es möglich, eine auf das Gebäude angepasste Betriebsführungsstrategie für die Bauteilaktivierung zu finden und einheitlich zu bewerten.
Asynchronmaschinen mit Kaefiglaeufer benoetigen waehrend ihres Hochlaufs das 3- bis 8fache des Bemessungsstroms. Dieser hohe Anlaufstrom geht erst zurueck, wenn der Kippschlupf erreicht ist (bei etwa 90% der Bemessungsdrehzahl). Wenn die Kurzschlussleistung des einspeisenden Netzes zum Zeitpunkt der Motorzuschaltung gering ist, koennen durch Spannungseinbrueche Anlaufprobleme einer Kaefiglaeufermaschine auftreten. Bei der Planung eines solchen Antriebs muessen deshalb genauere Simulationsrechnungen ueber die Zusammenhaenge von Hochlaufzeit, Spannungseinbruch und zulaessigen Grenzwerten durchgefuehrt werden. Ergebnisse derartiger Anlaufsimulationen eines 800-kW- und eines 1,13-MW-Hochspannungsmotors bei Anschaltung an einen 10-MVA- und einen 2-MVA-Generator wurden fuer verschiedene Zuschaltungssituationen in Oszillogrammen festgehalten. Durch genauere mathematische Angaben verdeutlicht werden die Faelle des Motorhochlaufs bei Inselbetrieb mit geringer Kurzschlussleistung sowie die Zuschaltung der Asynchronmotoren auf den Generator vor und nach Anhebung der Netzspannung behandelt. Angaben werden ferner gemacht zur Zuschaltung des 1,13-MW-Motors auf die Parallelschaltung des 10-MVA- und des 2-MVA-Generators. Aus den Simulationsoszillogrammen der Faelle von Hochlauf und Motorzuschaltung sind die zeitabhaengigen Aenderungen von Ankerstrom, Wirkleistungsaufnahme, Blindleistungsaufnahme, Klemmenspannung, Drehzahlabweichung, Antriebsmoment und Lastdrehmoment zu entnehmen.
In the present study, in vitro toxicity as well as biopersistence and photopersistence of four artificial sweeteners (acesulfame, cyclamate, saccharine, and sucralose) and five antibiotics (levofloxacin, lincomycin, linezolid, marbofloxacin, and sarafloxacin) and of their phototransformation products (PTPs) were investigated. Furthermore, antibiotic activity was evaluated after UV irradiation and after exposure to inocula of a sewage treatment plant. The study reveals that most of the tested compounds and their PTPs were neither readily nor inherently biodegradable in the Organisation for Economic Co-operation and Development (OECD)-biodegradability tests. The study further demonstrates that PTPs are formed upon irradiation with an Hg lamp (UV light) and, to a lesser extent, upon irradiation with a Xe lamp (mimics sunlight). Comparing the nonirradiated with the corresponding irradiated solutions, a higher chronic toxicity against bacteria was found for the irradiated solutions of linezolid. Neither cytotoxicity nor genotoxicity was found in human cervical (HeLa) and liver (Hep-G2) cells for any of the investigated compounds or their PTPs. Antimicrobial activity of the tested fluoroquinolones was reduced after UV treatment, but it was not reduced after a 28-day exposure to inocula of a sewage treatment plant. This comparative study shows that PTPs can be formed as a result of UV treatment. The study further demonstrated that UV irradiation can be effective in reducing the antimicrobial activity of antibiotics, and consequently may help to reduce antimicrobial resistance in wastewaters. Nevertheless, the study also highlights that some PTPs may exhibit a higher ecotoxicity than the respective parent compounds. Consequently, UV treatment does not transform all micropollutants into harmless compounds and may not be a large-scale effluent treatment option.
Bei thermischen Konvektionsströmungen ist der Einfluß von Geometrie und Randbedingungen für die Strömungsform und den konvektiven Wärmetransport von wesentlicher Bedeutung. Mit Hilfe der optischen Strömungsmeßtechnik (Differentialinterferometrie) wurde die freie Konvektion in einem quaderförmigen Behälter mit seitlicher Beheizung untersucht. Der Aufbau und die Experimente werden beschrieben. Die quantitative Auswertung von Dichte- und Temperaturfeldern aus den Differentialinterferogrammen wird aufgezeigt und der Einfluß unterschiedlicher Randbedingungen wie feste und freie Oberfläche auf die Strömungsform und den Wärmetransport dargelegt. Die eingesetzte Differentialinterferometrie zeigt aufgrund ihrer Anpassungsfähigkeit an die jeweiligen Versuchsbedingungen und durch den einfachen Aufbau spezifische Vorteile gegenüber dem Mach-Zehnder Interferometer.
Cooling towers or recoolers are one of the major consumers of electricity in a HVAC plant. The implementation and analysis of advanced control methods in a practical application and its comparison with conventional controllers is necessary to establish a framework for their feasibility especially in the field of decentralised energy systems. A standard industrial controller, a PID and a model based controller were developed and tested in an experimental set-up using market-ready components. The characteristics of these controllers such as settling time, control difference, and frequency of control actions are compared based on the monitoring data. Modern controllers demonstrated clear advantages in terms of energy savings and higher accuracy and a model based controller was easier to set-up than a PID.
Today, thermoforming moulds are mostly produced using conventional mould-building technologies (e.g. milling and drilling) and are made of metal (e.g. aluminium or steel) or hardwood. The tools thus produced are very robust, but are only cost-effective in mass production. For the production of small batches of thermoformed parts, there is a need for moulds which can be produced quickly and economically. A new approach which significantly reduces the production time and cost is the 3D printing process (3DP). The use of this technology to produce thermoforming moulds offers many new options in the geometries which can be manufactured, and in manufacturing time and costs. In a case study of a thermoformed part (a scaled automotive model), the pre-processing of the CAD model of a mould is demonstrated. The mould can be printed within a few hours, and is sufficiently heat-resistant for moulding processes. The important advantages of moulds printed in 3D, in comparison to moulds built using conventional technologies, are the ability to create any shape of channels for the vacuum and the simplification in the production of tool mock-ups. This paper also discusses the economics of the technique, such as a comparison of material costs and manufacturing costs in relation to conventional production technologies and materials.
Cast aluminum cylinder blocks are frequently used in gasoline and diesel internal combustion engines because of their light-weight advantage. However, the disadvantage of aluminum alloys is their relatively low strength and fatigue resistance which make aluminum blocks prone to fatigue cracking. Engine blocks must withstand a combination of low-cycle fatigue (LCF) thermal loads and high-cycle fatigue (HCF) combustion and dynamic loads. Reliable computational methods are needed that allow for accurate fatigue assessment of cylinder blocks under this combined loading. In several publications, the mechanism-based thermomechanical fatigue (TMF) damage model DTMF describing the growth of short fatigue cracks has been extended to include the effect of both LCF thermal loads and superimposed HCF loadings. This approach is applied to the finite life fatigue assessment of an aluminum cylinder block. The required material properties related to LCF are determined from uniaxial LCF tests. The additional material properties required for the assessment of superimposed HCF are obtained from the literature for similar materials. The predictions of the model agree well with engine dyno test results. Finally, some improvements to the current process are discussed.
4D printing (4DP) is an evolutionary step of 3D printing, which includes the fourth dimension, in this case the time. In different time steps the printed structure shows different shapes, influenced by external stimuli like light, temperature, pH value, electric or magnetic field. The advantage of 4DP is the solution of technical problems without the need for complex internal energy supply via cables or pipes. Previous approaches to 4D printing with magnetoresponsive materials only use materials with limited usability (e.g. hydrogels) and complex programming during the manufacturing process (e.g. using magnets on the nozzle). The 4D printing using unmagnetized particles and the later magnetization allows the use of a standard 3D printer and has the advantage of being easily reproducible and relatively inexpensive for further application. Therefore, a magnetoresponsive feedstock filament is produced which shows elastic and magnetic properties. In a first step, pellets are produced by compounding polymer with magnetic particles. In a second step, those pellets are extruded in form of filament. This filament is printed using a conventional printing system for Material Extrusion (MEX-TRB/P). Various prototypes have been printed, deformed and magnetized, which is called programming. In comparison to shape memory polymers (SMP) the repeatability of the movement is better. The results show the possibilities of application and function of magnetoresponsive materials. In addition, an understanding of the behaviour of this novel material is achieved.
More than 200 years ago, the scientist Alexander von Humboldt noted in his travel diaries that "everything is interconnectedness", when he was fascinated by nature and the phenomena observed. The view of nature has become much more detailed through the knowledge of phenomena and natural processes, which led to a more precise view of nature shaped by Humboldt. Technological progress and the artificial intelligence of highly developed computer systems are upsetting this view and changing the established world view through a new, unprecedented interaction between man and machinery. Thus we need digital axioms and comprehensive rules and laws for such autonomous acting systems that determine human interaction between cybernetic systems and biological individuals. This digital humanism should encompass our relationship to nature, our handling of the complexity and diversity of nature and the technological influences on society in order to avoid technical colonialism through supercomputers.
In this paper fatigue crack closure under in-phase and out-of-phase thermomechanical fatigue (TMF) loading is studied using a temperature dependent strip yield model. It is shown that fatigue crack closure is strongly influenced by the phase relation between mechanical loading and temperature, if the temperature difference goes along with a temperature dependence of the yield stress. In order to demonstrate the effect of the temperature dependent yield stress, the influence of in-phase and out-of-phase TMF loading is studied for a polycrystalline nickel-base superalloy. By using a mechanism based lifetime model, implications for fatigue lives are demonstrated.
As a basis for the evaluation of hydrogen storage by physisorption, adsorption isotherms of H2 were experimentally determined for several porous materials at 77 K and 298 K at pressures up to 15 MPa. Activated carbons and MOFs were studied as the most promising materials for this purpose. A noble focus was given on how to determine whether a material is feasible for hydrogen storage or not, dealing with an assessment method and the pitfalls and problems of determining the viability. For a quantitative evaluation of the feasibility of sorptive hydrogen storage in a general analysis, it is suggested to compare the stored amount in a theoretical tank filled with adsorbents to the amount of hydrogen stored in the same tank without adsorbents. According to our results, an “ideal” sorbent for hydrogen storage at 77 K is calculated to exhibit a specific surface area of >2580 m2 g−1 and a micropore volume of >1.58 cm3 g−1.
To improve the building’s energy efficiency many parameters should be assessed considering the building envelope, energy loads, occupation, and HVAC systems. Fenestration is among the most important variables impacting residential building indoor temperatures. So, it is crucial to use the most optimal energy-efficient window glazing in buildings to reduce energy consumption and at the same time provide visual daylight comfort and thermal comfort. Many studies have focused on the improvement of building energy efficiency focusing on the building envelope or the heating, ventilation, and cooling systems. But just a few studies have focused on studying the effect of glazing on building energy consumption. Thus, this paper aims to study the influence of different glazing types on the building’s heating and cooling energy consumption. A real case study building located under a semi-arid climate was used. The building energy model has been conducted using the OpenStudio simulation engine. Building indoor temperature was calibrated using ASHRAE’s statistical indices. Then a comparative analysis was conducted using seven different types of windows including single, double, and triple glazing filled with air and argon. Tripleglazed and double-glazed windows with argon space offer 37% and 32% of annual energy savings. It should be stressed that the methodology developed in this paper could be useful for further studies to improve building energy efficiency using optimal window glazing.
Die erste Auflage von "Ausführung von Stahlbauten" wurde – trotz ihres erheblichen Umfangs – zu einem sehr beliebten Nachschlagewerk und unverzichtbaren Praxishelfer in vielen Bereichen des Stahlbaus. Nachdem die Normen, auf die sich die erste Auflage bezieht, grundlegend überarbeitet wurden, entstand mit dem hier vorliegenden Buch auch eine aktualisierte Nachfolgeausgabe der Kommentare. Das Werk profitiert davon, dass es von den im Normungsausschuss federführenden Spezialisten ausgearbeitet wurde: Die Autoren liefern also zuverlässig die korrekten Interpretationen der Normentexte. Damit ist auch diese zweite Auflage von "Ausführung von Stahlbauten" eine gute Wahl, um mit den Normen DIN EN 1090-2 und DIN EN 1090-4 sicher und professionell arbeiten zu können. Da sich die Norm DIN EN 1090-1 aktuell in Überarbeitung befindet, ist diese nicht Teil der zweiten Auflage der Stahlbauten-Kommentare.
Der Bericht beschreibt die Vorgehensweise für die Entwicklung von Hochleistungszweitaktmotoren beim Institut für Transportwesen und Motorentechnik (ITM). Die gezielte Auswertung von motorischen Daten bietet die Möglichkeit, Motorenentwicklungsprozesse in wichtigen Fragestellung zu unterstützen. Für die Auslegung von Bauteilen und Prozessen werden Simulationsprogramme eingesetzt. Diese Entwicklungswerkzeuge können effizienter angewandt werden, wenn die Berechnungsergebnisse einer Qualitätskontrolle unterliegen. Wichtig hierfür sind Bewertungskriterien, die aus der Erfahrung einer Vielzahl von Versuchen bestehen. Da in Produktion gegangene Motoren üblicherweise schon einen Evolutionsprozeß durchlaufen haben, kann vermutet werden, daß solche Kriterien von erfolgreichen und weniger erfolgreichen Produkten in der Weise abgeleitet werden können, wie dies hier vorgestellt wurde. Die Angabe von Trendfunktionen für konstruktive Merkmale und Betriebsparameter ist notwendig um eine bedarfsorientierte Vorauslegung von Antrieben durchführen zu können. Alle hier vorgestellten Ergebnisse sind natürlich von der Datenmenge abhängig, die zu den jeweiligen Fragestellungen ausgewertet werden kann. Dazu müssen alle durchgeführten Versuchsreihen in die Datenbank eingeführt und mit Ergebnissen der Simulationsrechnungen in Beziehung gesetzt werden.
Automatic Identification of Travel Locations in Rare Books - Object Oriented Information Management
(2017)
The digital content of the Internet is growing exponentially and mass digitization of printed media opens access to literature, in particular the genre of travel literature from the 18th and 19th century, which consists of diaries or travel books describing routes, observations or inspirations. The identification of described locations in the digital text is a long-standing challenge which requires information technology to supply dynamic links to sources by new forms of interaction and synthesis between humanistic texts and scientific observations.
Using object oriented information technology, a prototype of a software tool is developed which makes it possible to automatically identify geographic locations and travel routes mentioned in rare books. The information objects contain properties such as names and classification codes for populated places, streams, mountains and regions. Together, with the latitudes and longitudes of every single location, it is possible to geo-reference this information in order that all processed and filtered datasets can be displayed by a map application. This method has already been used in the Humboldt Digital Library to present Alexander von Humboldt’s maps and was tested in a case study to prove the correctness and reliability of the automatic identification of locations based on the work of Alexander von Humboldt and Johann Wolfgang von Goethe.
The results reveal numerous errors due to misspellings, change of location names, equality of terms and location names. But on the other hand it becomes very clear that results of the automatic object detection and recognition can be improved by error-free and comprehensive sources. As a result an increase in quality and usability of the service can be expected, accompanied by more options to detect unknown locations in the descriptions of rare books.
Automation devices or automation stations (AS) take on the task of controlling, regulating, monitoring and, if necessary, optimising building systems and their system components (e.g. pumps, compressors, fans) based on recorded process variables. For this purpose, a wide range of control and regulation methods are used, starting with simple on/off controllers, through classic PID controllers, to higher-order controllers such as adaptive, model-predictive, knowledge-based or adaptive controllers.
Starting with a brief introduction to automation technology (Sect. 7.1), the chapter goes into the structure and functionality of the usual compact controllers using the application examples of solar thermal systems and heat pump systems (Sect. 7.2). Finally, the integration of system automation into a higher-level building automation system and into the building management system is described using specific application examples (Sect. 7.3).
This central book chapter now details the implementation of automation of solar domestic hot water systems, solar assisted building heating, rooms, solar cooling systems, heat pump heating systems, geothermal systems and thermally activated building component systems. Hydraulic and automation diagrams are used to explain how the automation of these systems works. A detailed insight into the engineering and technical interrelationships involved in the use of these systems, as well as the use of simulation tools, enables effective control and regulation. System characteristic curves and systematic procedures support the automation engineer in his tasks.
Cyclic micro-bending tests on fcc single crystal Ni-base Alloy 718 cantilevers with different crystal orientations were performed to analyze the influence of activated slip systems on dislocation plasticity, latent hardening and the Bauschinger effect. The investigations indicate that plasticity in single crystal micro-cantilevers is significantly influenced by two phenomena - dislocation interaction and dislocation pile-up at the neutral plane. Both phenomena occur at the same time. Their ratio seems to be determined by the activated slip systems. Slip trace analysis indicates that the activation of only one slip system leads to a strong localization of plasticity to a limited number of parallel slip bands. This results in low dislocation interaction and consequently pronounced pile-ups at the neutral plane. In multi slip orientation, the second slip system leads to activation of significantly more dislocation sources, causing a much earlier and more homogeneous elastic-plastic transition zone. In stress-strain hysteresis loops during bending, pronounced dislocation interaction in multi slip orientation leads to a more pronounced latent hardening. The results suggest that on a microstructural length scale, plasticity behavior is strongly affected by activated slip systems, which determine local dislocation phenomena. Based on the results presented in this paper, a finite element analysis of latent hardening and the Bauschinger effect using a single crystal plasticity model with latent kinematic hardening is presented in Part II.
In this paper, the Bauschinger effect and latent hardening of single crystals are assessed in finite element calculations using a single crystal plasticity model with kinematic hardening. To this end, results of cyclic micro-bending experiments on single crystal Alloy 718 in different crystal orientations (single slip and multi slip) with respect to the loading direction are used to determine the slip system related material properties of the single crystal plasticity model. Two kinematic hardening laws are considered: a kinematic hardening law describing latent hardening and a kinematic hardening law without latent hardening. For the determination of material properties for both hardening laws, a gradient-based optimization method is used. The results show that the different strength levels observed for micro-bending tests on different crystal orientations can only be described with latent kinematic hardening well, whereas the pronounced Bauschinger effect is described well by both kinematic hardening laws. It is concluded that cyclic micro-bending experiments on single crystals using different crystal orientations give an appropriate data base for the determination of the slip system related material properties of the single crystal plasticity model with latent kinematic hardening.
Bauteilaktivierung
(2015)
Digital libraries are providing an increasing amount of data, which is normally structured in a classical way by documents and described by metadata as keywords. The data, even in scientific systems such as digital libraries and virtual research environments, will contain a great amount of noise or information unnecessary for our personal interests. Although there has been a lot of progress in the field of information retrieval, search techniques and other content finding methods, there is still much to be done in the field of information retrieval based on user behavior. This paper presents an approach deployed in the Humboldt Digital Library (HDL) to facilitate the retrieval of relevant information to the users of the system, making recommendations of paragraphs based on their profile and the behavior of other users who share similar profiles. The Humboldt digital library represents an innovative system of open access to the legacy of Alexander von Humboldt in a digital form on the Internet (www.avhumboldt.net). It contributes to the key question, how to present interconnected data in a proper form using information technologies.
In the modern knowledge-based and digital economy, the value of knowledge is growing relative to other assets and new intellectual property is being created at an ever-increasing rate. Therefore, the ability to find non-trivial solutions, systematically generate new concepts, and create intellectual property rapidly become crucial to achieving competitive advantage and leveraging the intellectual potential of organizations.