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The research employed HPTLC Pro System and other HPTLC instruments from CAMAG® to conduct various laboratory tests, aiming to compile a database for subsequent analyses. Utilizing MATLAB, distinct codes were developed to reveal patterns within analyzed biomasses and pyrolysis oils (sewage sludge, fermentation residue, paper sludge, and wood). Through meticulous visual and numerical analysis, shared characteristics among different biomasses and their respective pyrolysis oils were revealed, showcasing close similarities within each category. Notably, minimal disparity was observed in fermentation residue and wood biomasses with a similarity coefficient of 0.22. Similarly, for pyrolysis oils, the minimal disparity was found in fermentation residues 1 and 3, with a disparity coefficient of 1.41. Despite higher disparity coefficients in certain results, specific biomasses and pyrolysis oils, such as fermentation residue and sewage sludge, exhibited close similarities, with disparity coefficients of 0.18 and 0.55, respectively. The database, derived from triplicate experimentation, now serves as a valuable resource for rapid analysis of newly acquired raw materials. Additionally, the utility of HPTLC PRO as an investigation tool, enabling simultaneous analysis of up to five samples, was emphasized, although areas for improvement in derivatization methods were identified.
In the field of network security, the detection of intrusions is an important task to prevent and analyse attacks.
In recent years, an increasing number of works have been published on this subject, which perform this detection based on machine learning techniques.
Thereby not only the well-studied detection of intrusions, but also the real-time capability must be considered.
This thesis addresses the real-time functionality of machine learning based network intrusion detection.
For this purpose we introduce the network feature generator library PyNetFlowGen, which is designed to allow real-time processing of network data.
This library generates 83 statistical features based on reassembled data flows.
The introduced performant Cython implementation allows processing individual packets within 4.58 microseconds.
Based on the generated features, machine learning models were examined with regard to their runtime and real-time capabilities.
The selected Decision-Tree-Classifier model created in Python was further optimised by transpiling it into C-Code, what reduced the prediction time of a single sample to 3.96 microseconds on average.
Based on the feature generator and the machine learning model, an basic IDS system was implemented, which allows a data throughput between 63.7 Mbit/s and 2.5 Gbit/s.