Refine
Year of publication
- 2005 (13) (remove)
Document Type
Conference Type
- Konferenzartikel (4)
- Sonstiges (2)
- Konferenz-Abstract (1)
Language
- English (13) (remove)
Has Fulltext
- no (13) (remove)
Is part of the Bibliography
- yes (13)
Keywords
- Applied computing (1)
- Benzodiazepine (1)
- E-learning (1)
- Education (1)
- Gerichtliche Chemie (1)
- HCI (1)
- Human computer interaction (1)
- Human-centered computing (1)
- Pharmazie (1)
- Thin layer chromatography (1)
Institute
Open Access
- Closed Access (7)
- Open Access (3)
- Closed (1)
The goal of eLearning services integration in manufacturing is, through the development of new multimedia solutions, to accelerate and enhance the ability of the manufacturing industry to capitalise on the emergence of a powerful global information infrastructure. The key components of our approach are: (1) an XML based streaming service specification language; (2) automatic configuration of distributed eLearning streaming service implementations; (3) a set of Web services for searching, registration, and creation of streaming services; (4) caching and replication policies based on timing information derived from the service specifications. We also introduce a new concept for cache management during runtime, e.g., content is distributed to cache servers located at the edge of a network close to the client.
Diode-array planar chromatography is a versatile tool for identification of pharmaceutical substances In this paper thirty-three compounds with benzodiazepine properties were investigated and the separating conditions for silica gel HPTLC plates and three mobile phases were optimized. Diode-array HPTLC makes it possible to identify all the compounds with high certainty down to a level of 20 ng. An algorithm for spectral recognition which is combined with R F values from the three separation steps into one fit factor is presented. This set of data is unique for each of the compounds investigated and enables unequivocal identification. The method is rapid, inexpensive, and sensitive down to a level of 20 ng mL −1.
Specific prototypes of sedimentation field flow fractionation devices (SdFFF) have been developed with relative success for cell sorting. However, no data are available to compare these apparatus with commercial ones. In order to compare with other devices mainly used for non-biological species, biocompatible systems were used for standard particle (latex: 3–10 μm of different size dispersities) separation development. In order to enhance size dependent separations, channels of reduced thickness were used (80 and 100 μm) and channel/carrier-phase equilibration procedures were necessary. For sample injection, the use of inlet tubing linked to the FFF accumulation wall, common for cell sorting, can be extended to latex species when they are eluted in the Steric Hyperlayer elution mode. It avoids any primary relaxation steps (stop flow injection procedure) simplifying series of elution processing. Mixtures composed of four different monodispersed latex beads can be eluted in 6 min with 100 μm channel thickness.
The three wavelength extinction method (3-WEM) was applied for the on-line particle analysisof suspensions of monodisperse latex beads and polydisperse metal oxide particles of industrialinterest. Comparative measurements were performed by photon correlation spectroscopy (PCS). Thedata of latex particles obtained by 3-WEM and PCS are in good agreement with the manufacture’svalues. Also, the values of oxide particles measured by means of the two techniques are in reasonableagreement despite of the irregular particle shape.Discrepancies are observed by comparing the oxideparticle size results with those of scanning electron microscopy, which is due to the broad sampledistributions and shape irregularities.
Thin-layer chromatography (TLC) is a well-established and widely used separation technique. Most undergraduate students of chemistry or food science used TLC as a primitive separation tool, which does not need more than small pieces of TLC plates, a glass jar and some solvents. TLC has evolved from a simple separation method of the past into an instrumental technique that offers automation, reproducibility and accurate quantification for a wide variety of applications [1]. The use of modern 10*10 cm TLC plates with narrow particle size distribution is called high performance thin layer chromatography (HPTLC), to distinguish the method from the use of traditional 20 20 cm TLC plates.