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Monitoring of the molecular structure of lubricant oil using a FT-Raman spectrometer prototype
(2014)
The determination of the physical state of the lubricant materials in complex mechanical systems is highly critical from different points of view: operative, economical, environmental, etc. Furthermore, there are several parameters that a lubricant oil must meet for a proper performance inside a machine. The monitoring of these lubricants can represent a serious issue depending on the analytical approach applied. The molecular change of aging lubricant oils have been analyzed using an all-standard-components and self-designed FT-Raman spectrometer. This analytical tool allows the direct and clean study of the vibrational changes in the molecular structure of the oils without having direct contact with the samples and without extracting the sample from the machine in operation. The FT-Raman spectrometer prototype used in the analysis of the oil samples consist of a Michelson interferometer and a self-designed photon counter cooled down on a Peltier element arrangement. The light coupling has been accomplished by using a conventional 62.5/125μm multi-mode fiber coupler. The FT-Raman arrangement has been able to extract high resolution and frequency precise Raman spectra, comparable to those obtained with commercial FT-Raman systems, from the lubricant oil samples analyzed. The spectral information has helped to determine certain molecular changes in the initial phases of wearing of the oil samples. The proposed instrument prototype has no additional complex hardware components or costly software modules. The mechanical and thermal irregularities influencing the FT-Raman spectrometer have been removed mathematically by accurately evaluating the optical path difference of the Michelson interferometer. This has been achieved by producing an additional interference pattern signal with a λ= 632.8 nm helium-neon laser, which differs from the conventional zero-crossing sampling (also known as Connes advantage) commonly used by FT-devices. It enables the FT-Raman system to perform reliable and clean spectral measurements from the analyzed oil samples.
Besonderes Außensteuerrecht
(2014)
Signal detection and bandwidth estimation, also known as channel segmentation or information channel estimation, is a perpetual topic in communication systems. In the field of radio monitoring this issue is extremely challenging, since unforeseeable effects like fading occur accidentally. In addition, most radio monitoring devices normally scan a wide frequency range of several hundred MHz and have to detect a multitude of different signals, varying in signal power, bandwidth and spectral shape. Since narrowband sensing techniques cannot be directly applied, most radio monitoring devices use Nyquist wideband sensing to discover the huge frequency range. In practice, sensing is normally conducted by an FFT sweep spectrum analyzer that delivers the power spectral density (PSD) values to the radio monitoring system. The channel segmentation is the initial step of a comprehensive signal analysis in a radio monitoring system based on the PSD values. In this paper, a novel approach for channel segmentation is presented that is based on a quantization and a histogram evaluation of the measured PSD. It will be shown that only the combination of both evaluations will lead to an successful automatic channel segmentation. The performance of the proposed algorithm is shown in a real radio monitoring szenario.