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Quantification of astaxanthin in salmons by chemiluminescence and absorption after TLC separation
(2018)
Astaxanthin is a keto-carotenoid, belongs to the chemical class of terpenes and is a yellow lipid soluble compound. The compound is present in marine animals like salmons and crustacean. Its colour is due to conjugated double bonds and these double bonds are responsible for its antioxidant effect. Its antioxidant activity is ten times stronger than other carotenoids and nearly 500 fold stronger than vitamin-E. We present a new thin layer chromatography (TLC) method to measure astaxanthin on TLC-plates (Merck, 1.05554) in the visible absorption range as well as by using chemiluminescence. For separation a solvent mixture of cyclohexane and acetone (10 + 2.4, v/v) was used. The RF-value of astaxanthin is 0.14.The limit of detection in vis-absorption is 64 ng / band and the limit of quantification is 92 ng/band. In chemiluminescence the values are 90 ng / band and 115 ng/band. The method offers two independently working measurement modes on a single plate which increase the accuracy of the quantification.
The authors claim that location information of stationary ICT components can never be unclassified. They describe how swarm-mapping crowd sourcing is used by Apple and Google to worldwide harvest geo-location information on wireless access points and mobile telecommunication systems' base stations to build up gigantic databases with very exclusive access rights. After having highlighted the known technical facts, in the speculative part of this article, the authors argue how this may impact cyber deterrence strategies of states and alliances understanding the cyberspace as another domain of geostrategic relevance. The states and alliances spectrum of activities due to the potential existence of such databases may range from geopolitical negotiations by institutions understanding international affairs as their core business, mitigation approaches at a technical level, over means of cyber deterrence-by-retaliation.
In a Semi-autonomic cloud auditing architecture we weaved in privacy enhancing mechanisms [15] by applying the public key version of the Somewhat homomorphic encryption (SHE) scheme from [4]. It turns out that the performance of the SHE can be significantly improved by carefully deriving relevant crypto parameters from the concrete cloud auditing use cases for which the scheme serves as a privacy enhancing approach. We provide a generic algorithm for finding good SHE parameters with respect to a given use case scenario by analyzing and taking into consideration security, correctness and performance of the scheme. Also, to show the relevance of our proposed algorithms we apply it to two predominant cloud auditing use cases.
Covert- and side-channels as well as techniques to establish them in cloud computing are in focus of research for quite some time. However, not many concrete mitigation methods have been developed and even less have been adapted and concretely implemented by cloud providers. Thus, we recently conceptually proposed C 3 -Sched a CPU scheduling based approach to mitigate L2 cache covert-channels. Instead of flushing the cache on every context switch, we schedule trusted virtual machines to create noise which prevents potential covert-channels. Additionally, our approach aims on preserving performance by utilizing existing instead of artificial workload while reducing covert-channel related cache flushes to cases where not enough noise has been achieved. In this work we evaluate cache covert-channel mitigation and performance impact of our integration of C 3 -Sched in the XEN credit scheduler. Moreover, we compare it to naive solutions and more competitive approaches.
A simple measuring method for acquiring the radiation pattern of an ultrawide band Vivaldi antenna is presented. The measuring is performed by combining two identical Vivaldi antennas and some of the intrinsic properties of a stepped-frequency continue wave radar (SFCW radar) in the
range from 1.0 GHz to 6.0 GHz. A stepper-motor provided the azimuthal rotation for one of the antennas from 0 ◦ to 360 ◦. The tests have been performed within the conventional environment (laboratory / office) without using an anechoic chamber or absorbing materials. Special measuring devices have not been used either. This method has been tested with different pairs of Vivaldi antennas and it can be also used for different ones (with little or no change in the system), as long as their operational
bandwidth is within the frequency range of the SFCW radar.
Keywords — SFCW Radar, Antenna Gain Characterization,
Azimuthal Radiation Pattern
In this paper, we establish a simple model for the exchange of messages in a vehicular network and we consider fundamental limits on the achievable data rate. For a vehicular network, the exchange of data with other nearby vehicles is particularly important for traffic safety, e.g. for collision avoidance, but also for cooperative applications like platooning. These use cases are currently addressed by standards building on IEEE 802.11p, namely ITS-G5 and DSRC (dedicated short range communication), which encounter saturation problems at high vehicle densities. For this reason, we take a step back and ask for the fundamental limits for the common data rate in a vehicular network. After defining a simple single-lane model and the corresponding capacity limits for some basic multiple- access schemes, we present results for a more realistic setting. For both scenarios, non-orthogonal multiple-access (NOMA) yields the best results.
This paper evaluates the implementation of Medium Access Control (MAC) protocols suitable for massive access connectivity in 5G multi-service networks. The access protocol extends multi-packet detection receivers based on Physical Layer Network Coding (PLNC) decoding and Coded Random Access protocols considering practical aspects to implement one-stage MAC protocols for short packet communications in mMTC services. Extensions to enhance data delivery phase in two- stage protocols are also proposed. The assessment of the access protocols is extended under system level simulations where a suitable link to system interface characterization has been taken into account.
Micro-cracks give rise to non-analytic behavior of the stress-strain relation. For the case of a homogeneous spatial distribution of aligned flat micro-cracks, the influence of this property of the stress-strain relation on harmonic generation is analyzed for Rayleigh waves and for acoustic wedge waves with the help of a simple micromechanical model adopted from the literature. For the efficiencies of harmonic generation of these guided waves, explicit expressions are derived in terms of the corresponding linear wave fields. The initial growth rates of the second harmonic, i.e., the acoustic nonlinearity parameter, has been evaluated numerically for steel as matrix material. The growth rate of the second harmonic of Rayleigh waves has also been determined for microcrack distributions with random orientation, using a model expression for the strain energy in terms of strain invariants known in a geophysical context.
For an elastic medium containing a homogeneous distribution of micro-cracks, an effective one-dimensional stress-strain relation has been determined with finite element simulations. In addition to flat micro-cracks, voids were considered that contain a Hertzian contact, which represents an example for micro-cracks with internal structure. The orientation of both types of micro-cracks was fully aligned or, for flat micro-cracks, totally random. For micro-cracks with Hertzian contacts, the case of random orientation was treated in an approximate way. The two types of defects were found to give rise to different degrees of non-analytic behavior of the effective stress-strain relation, which governs the nonlinear propagation of symmetric (S0) Lamb waves in the long-wavelength limit. The presence of flat micro-cracks causes even harmonics to grow linearly with propagation distance with amplitudes proportional to the amplitude of the fundamental wave, and gives rise to a static strain. The presence of the second type of defects leads to a linear growth of all harmonics with amplitudes proportional to the power 3/2 of the fundamental amplitude, and to a strain-dependent velocity shift. Simple expressions are given for the growth rates of higher harmonics of S0 Lamb waves in terms of the parameters occurring in the effective stress-strain relation. They have partly been determined quantitatively with the help of the FEM results for different micro-crack concentrations.
Among the various types of guided acoustic waves, acoustic wedge waves are non-diffractive and non-dispersive. Both properties make them susceptible to nonlinear effects. Investigations have recently been focused on effects of second-order nonlinearity in connection with anisotropy. The current status of these investigations is reviewed in the context of earlier work on nonlinear properties of two-dimensional guided acoustic waves, in particular surface waves. The role of weak dispersion, leading to solitary waves, is also discussed. For anti-symmetric flexural wedge waves propagating in isotropic media or in anisotropic media with reflection symmetry with respect to the wedge’s mid-plane, an evolution equation is derived that accounts for an effective third-order nonlinearity of acoustic wedge waves. For the kernel functions occurring in the nonlinear terms of this equation, expressions in terms of overlap integrals with Laguerre functions are provided, which allow for their quantitative numerical evaluation. First numerical results for the efficiency of third-harmonic generation of flexural wedge waves are presented.
This paper is discussing the development of a wireless Indoor Smart Gardening System with the focus on energy autonomous working. The Smart Gardening System, which is presented in this paper consists of a network of energy autonomous wireless sensor nodes which are used for monitoring important plant parameters like air temperature, soil moisture, pressure or humidity and in future to control an actuator for the plant irrigation and to measure further parameter as light and fertilizer level. Solar energy harvesting is used for powering the wireless nodes without the usage of a battery. Comparable Smart Gardening Systems are usually battery-powered. Furthermore, the overall Smart Gardening System consists of a battery powered gateway based on a Raspberry Pi 3 system, which controls the wireless nodes and collects their sensor data. The gateway is able to send the information to an internet server application and via Wi-Fi to mobile devices. Particularly the architecture of the energy autonomous wireless nodes will be considered because fully energy autonomous wireless networks could not be implemented without special concepts for the energy supply and architecture of the wireless nodes.
Nowadays, robotic systems are an integral part of many orthopedic interventions. Stationary robots improve the accuracy but also require adapted surgical workflows. Handheld robotic devices (HHRDs), however, are easily integrated into existing workflows and represent a more economical solution. Their limited range of motion is compensated by the dexterity of the surgeon. This work presents control algorithms for HHRDs with multiple degrees of freedom (DOF). These algorithms protect pre- or intraoperatively defined regions from being penetrated by the end effector (e.g., a burr) by controlling the joints as well as the device’s power. Accuracy tests on a stationary prototype with three DOF show that the presented control algorithms produce results similar to those of stationary robots and much better results than conventional techniques. This work presents novel and innovative algorithms, which work robustly, accurately, and open up new opportunities for orthopedic interventions.
In rural low voltage grid networks, the use of battery in the households with a grid connected Photovoltaic (PV) system is a popular solution to shave the peak PV feed-in to the grid. For a single electricity price scenario, the existing forecast based control approaches together with a decision based control layer uses weather and load forecast data for the on–off schedule of the battery operation. These approaches do bring cost benefit from the battery usage. In this paper, the focus is to develop a Model Predictive Control (MPC) to maximize the use of the battery and shave the peaks in the PV feed-in and the load demand. The solution of the MPC allows to keep the PV feed-in and the grid consumption profile as low and as smooth as possible. The paper presents the mathematical formulation of the optimal control problem along with the cost benefit analysis . The MPC implementation scheme in the laboratory and experiment results have also been presented. The results show that the MPC is able to track the deviation in the weather forecast and operate the battery by solving the optimal control problem to handle this deviation.
Bei vielen Schulungen, Unterrichten und Weiterbildungen kommen PowerPoint-Präsentationen zum Einsatz, welche durch epische Länge, Unmengen von Informationen und Text charakterisiert sind. Zur Folge haben kann dies, dass die meisten Zuhörer binnen kürzester Zeit gedanklich abschalten, den Wortregen über sich ergehen lassen und dabei andere Dinge in den Fokus ihrer Aufmerksamkeit stellen. Die Autoren zeigen, wie und warum der »Zuhörer« zu einem »Zuschauer« werden sollte – sprich: die zu vermittelnden Aspekte und Informationen als einfache Bilder komprimiert darzustellen. Der folgende Beitrag setzt sich mit dieser Art von Perspektivenwechsel kontrovers auseinander und gibt für den Praxisalltag mögliche Lösungsansätze.