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Steroid hormones (SHs) are a rising concern due to their high bioactivity, ubiquitous nature, and prolonged existence as a micropollutants in water, they pose a potential risk to both human health and the environment, even at low concentrations. Estrogens, progesterone, and testosterone are the three important types of steroids essential for human development and maintaining multiorgan balance, are focus to this concern. These steroid hormones originate
from various sources, including human and livestock excretions, veterinary medications, agricultural runoff, and pharmaceuticals, contributing to their presence in the environment. According to the recommendation of WHO, the guidance value for estradiol (E2) is 1 ng/L. There are several methods been attempted to remove the SH micropollutant by conventional water and wastewater technologies which are still under research. Among the various methods, electrochemical membrane reactor (EMR) is one of the emerging technologies that can address the challenge of insufficient SHs removal from the aquatic environment by conventional treatment. The degradation of SHs can be significantly influenced by various factors when treated with EMR.
In this project, the removal of SH and the important mechanism for the removal using carbon nanotube CNT-EMR is studied and the efficiency of CNT-EMR in treating the SH micropollutant is identified. By varying different parameters this experiment is carried out with the (PES-CNTs) ultrafiltration membrane. The study is carried out depending upon the SH removal based on the limiting factor such as cell voltage, flux, temperature, concentration, and type of the SH.
Global energy demand is still on an increase during the last decade, with a lot of impact on the climate change due to the intensive use of conventional fossil-based fuels power plants to cover this demand. Most recently, leaders of the globe met in 2015 to come out with the Paris Agreement, stating that the countries will start to take a more responsible and effective behaviour toward the global warming and climate change issues. Many studies have discussed how the future energy system will look like with respecting the countries’ targets and limits of greenhouse gases and their CO2 emissions. However, these studies rarely discussed the industry sector in detail even though it is one of the major role players in the energy sector. Moreover, many studies have simulated and modelled the energy system with huge jumps of intervals in terms of years and environmental goals. In the first part of this study, a model will be developed for the German electrical grid with high spatial and temporal resolutions and different scenarios of it will be analysed meticulously on shorter periods (annual optimization), with different flexibilities and used technologies and degrees of innovations within each scenario. Moreover, the challenge in this research is to adequately map the diverse and different characteristics of the medium-sized industrial sector. In order to be able to take a first step in assessing the relevance of the industrial sector in Germany for climate protection goals, the industrial sector will be mapped in PyPSA-Eur (an open-source model data set of the European energy system at the level of the transmission network) by detailing the demand for different types of industry and assigning flexibilities to the industrial types. Synthetically generated load profiles of various industrial types are available. Flexibilities in the industrial sector are described by the project partner Fraunhofer IPA in the GaIN project and can be used. Using a scenario analysis, the development of the industrial sector and the use of flexibilities are then to be assessed quantitatively.
One of the main problematics of the seals tests is the time and money consuming they are. Up to now, there are few tries to do a digitalisation of a test where the seals behaviour can be known.
This work aims to digitally reproduce a seal test to extract their behaviour when working under different operation conditions to see their impact on the pimp’s efficiency. In this thesis, due to the Lomaking effect, the leakage and the forces applied on the stator will be the base of analysis.
First of all, among all the literature available for very different kind of seals and inner patterns, it has been chosen the most appropriate and precise data. The data chosen is “Test results for liquid Damper Seals using a Round-Hole Roughness Pattern for the Stator” from Fayolle, P. and “Static and Rotordynamic Characteristics of Liquid Annular Seals with Circumferentially/Grooved Stator and Smooth Rotor using three levels of circumferential Inlet-Fluid” from Torres J.M.
From the literature, dimensions of the test rig and the seals will be extracted to model them into a 3D CAD software. With the 3D CAD digitalisation, the fluid volumes for a rotor-centred position, meaning without eccentricity, will be extracted, and used. The following components have been modelled:
- Smooth Annular Liquid Seal (Grooved Rotor)
- Grooved Annular Liquid Seal (Smooth Rotor)
- Round-Hole Pattern Annular Liquid Seal (𝐻𝑑=2 𝑚𝑚) (Smooth Rotor)
- Straight Honeycomb Annular Liquid Seal (Smooth Rotor)
- Convergent Honeycomb Annular Liquid Seal (Smooth Rotor)
- Smooth Rotor / Smooth Annular Liquid Seal (Smooth Rotor)
As there is just one test rig, all the components have been adapted to the different dimensions of the seals by referencing some measures. This allows to test any seal with the same test rig.
Afterwards a CFD simulation that will be used to obtain leakage and stator forces. The parameters that will be changed are the rotational velocity of the fluid (2000 rpm, 4000 rpm, and 6000 rpm) and the pressure drop (2,068 bar, 4,137 bar, 6,205 bar, and 8,274 bar).
Those results will be compared to the literature ones, and they will determine if digitalisation can be validated or not. Even though the relative error is higher than 5% but the tendency is the same and it is thought that by changing some parameters the test results can be even closer to the literature ones.
The present document is aimed to propose a suitable thermal model for the cooling down process of a one piston air cooled reciprocating compressor. In order to achieve this, a thermographic camera is used to record the temperature of different measuring points throughout different operating conditions. This data is later analyzed, with statistical tools and graphical visualization. The thermal phenomena present in the thermal process is characterized according to the compressors' geometry. Finally, using the analysis and taking into consideration the thermal phenomena the optimal thermal model is selected. This paper belongs to a bigger project and the last step is to simulate the compressor and the accuracy of the proposed model.
Schluckspecht project
(2022)
To date, many experiments have been performed to study how the internal geometrical shapes of the annular liquid seal can reduce internal leakage and increase pump efficiency. These can be time-consuming and expensive as all rotordynamic coefficients must be determined in each case.
Nowadays, accurate simulation methods to calculate rotordynamic coefficients of annular seals are still rare. Therefore, new numerical methods must be designed and validated for annular seals.
The present study aims to contribute to this labour by providing a summary of the available test rig and seals dimensions and experimental results obtained in the following experiments:
− Kaneko, S et al., Experimental Study on Static and Dynamic Characteristics of Liquid Annular Convergent-Tapered Seals with Honeycomb Roughness Pattern (2003) [1] − J. Alex Moreland, Influence of pre-swirl and eccentricity in smooth stator/grooved rotor liquid annular seals, static and rotordynamic characteristics (2016) [2]
A 3D CAD simulation with Siemens NX Software of the test rig used in J. Alex Moreland’s experiment has been made. The following annular liquid seals have also been 3D modelled, as well as their fluid volume:
− Smooth Annular Liquid Seal (SS/GR) (J. Alex Moreland experiment)
− Grooved Annular Liquid Seal (GS/SR)
− Round-Hole Pattern Annular Liquid Seal (𝐻𝑑=2 mm) (GS/SR)
− Straight Honeycomb Annular Liquid Seal (GS/SR)
− Convergent Honeycomb Annular Liquid Seal (No. 3) (GS/SR)
− Smooth Annular Liquid Seal (SS/SR) (S. Kaneko experiment)
In the case of the seals used in S. Kaneko’s experiments, the test rig has been adapted to each seal, defining interpart expressions which can be easily modified.
Afterwards, it has been done a CFD simulation of the Smooth Annular Liquid Seal using Ansys CFX Software. To do so, the fluid volume geometry has been simplified to do a first approximation. Results have been compared for an eccentricity 𝜀0=0.00 for the following ranges of rotor speeds and differential of pressure:
− Δ𝑃= 2.07, 4.14, 6.21, and 8.27 bar,
− 𝜔= 2, 4, 6 and 8 krpm.
Even results obtained have the same trend as the one proportionated by the literature, they cannot be validated as the error is above 5%. It is also observed that as the pressure drop increases, the relative error decreases considerably.
The objective of this thesis is the quantification and qualification of neonicotinoid insecticides using thin-layer chromatography (TLC). Neonicotinoids are a relatively new form of pesticides, which have been proven to be extremely lethal to the honey bee, Apis mellifera. In this paper six forms of neonicotinoid insecticides (i.e. Acetamiprid, Thiacloprid, Imidacloprid, Clothianidin, Thaimethoxam, and Nitenpyram) are analysed. The initial steps are to first find a suitable mobile phase eluent, followed by the search for a reagent causing a luminescence effect of the neonicotinoids on a TLC plate. Subsequently, a calibration method is then used to find the detection limit of this TLC experiment. The aim is, therefore, to achieve a standard method of quantifying and qualifying neonicotinoids via TLC. Whilst a suitable mobile phase has been established, an optimal fluorescent reagent has yet to be found and more research on the subject must be carried out.
As the population grows, so does the amount of biowaste. As demand for energy grows, biogas is a promising solution to the problem. Lignocellulosic materials are challenged of slow degradability due to the presence of polymers such as cellulose, lignin and hemicellulose. There are several pretreatment methods available to enhance the degradability of such materials, including enzymatic pretreatment. In this pretreatment, there are few parameters that can influence the results, the most important being the enzyme to solid ratio and the solid to liquid ratio. During this project, experiments were conducted to determine the optimal conditions for those two factors. It was discovered that a solid to liquid ratio of 31 g of buffer per 1 gram of organic dry matter produced the highest reducing sugar release in flasks when combined with 34 mg of protein per 1 gram of organic dry mass. Additionally, another experiment was carried out to investigate the impact of enzymatic pretreatment on biogas production using artificial biowaste as a substrate. Artificial biowaste produced 577,9 NL/kg oDM, while enzymatically pretreated biowaste produced 639,3 NL/kg oDM. This resulted in a 10,6% rise in cumulative biogas production compared to its use without enzymatic pretreatment. By the conclusion of the investigation, specific cumulative dry methane yields of 364,7 NL/kg oDM and 426,3 NL/kg oDM were obtained from artificial biowaste without and with enzymatic pretreatment, respectively. This resulted in a methane production boost of 16,9%. Additionally in case of the reactors with enzymatically pretreated substrate kinetic constant was lower more than double, where maximum volume of biogas increased, comparing to the reactors without enzymatic pretreatment.
As society continues to age, the implementation of hip stems increases every year. However, there are a variety of different hip stem designs.
The aim of this project is to analyze which hip stem design implemented in a femur is most effective under different static loading conditions such as gait and sideways falling. In addition, a four-point-bending test was carried out. Therefore, the tech-niques were simulated in silico by FEA with Abaqus/CAE 2019.
A short stem, a straight stem and an anatomical stem were tested. All prosthesis are cementless press-fit stems. Each hip stem was examined in physiological and osteoporotic bone applying all three tests. To compare the stems the tests were also applied on a native bone model as a reference. Boundary conditions were used in order to simulate the tests.
The average von Mises stress, tension, compression and the risk of fracture were extracted and compared.
Biomechanical results show that the straight stem induces higher von Mises stresses compared to the anatomical stem. The risk of fracture is higher for osteo-porotic bone than for physiological bone. However, there is no risk of fracture as all the results are below the risk of value.
Decarbonisation Strategies in Energy Systems Modelling: Biochar as a Carbon Capture Technology
(2022)
The energy system is changing since some years in order to achieve the climate goals from the Paris Agreement which wants to prevent an increase of the global temperature above 2 °C. Decarbonisation of the energy system has become for governments a big challenge and different strategies are being stablished. Germany has set greenhouse gas reduction limits for different years and keeps track of the improvement made yearly. The expansion of renewable energy systems (RES) together with decarbonisation technologies are a key factor to accomplish this objective.
This research is done to analyse the effect of introducing biochar, a decarbonisation technology, and study how it will affect the energy system. Pyrolysis is the process from which biochar is obtained and it is modelled in an open-source energy system model. A sensibility analysis is made in order to assess the effect of changing the biomass potential and the costs for pyrolysis.
The role of pyrolysis is analysed in the form of different future scenarios to evaluate the impact. The CO2 emission limits from the years 2030 and 2045 are considered to create the scenarios, as well as the integration of flexibility technologies. Four scenarios in total are assessed and the result from the sensibility analysis considering pyrolysis are always compared to the reference scenario, where pyrolysis is not considered.
Results show that pyrolysis has a bigger impact in the energy system when the CO2 limit is low. Biochar can be used to compensate the emissions from other conventional power plant and achieve an energy transition with lower costs. Furthermore, it was also found that pyrolysis can also reduce the need of flexibility. This study also shows that the biomass potential and the pyrolysis costs can affect a lot the behaviour of pyrolysis in the energy system.
The Timed-Up-and-Go (TUG) test aims to assess mobility, balance, walking ability, and fall risk during walking. The instrumentalization of the TUG is already described in the literature and is beginning to be implemented in the industry. The products proposed by Zhortech and Digitsole, namely connected insoles, as well as additional sensors placed on the sternum and the right and eventually left femur allow the instrumentalization of the test.
An algorithm of detection and evaluation of the TUG has been developed in two versions. The first one (V1) aiming simply to calculate the total duration of the test. A second version is an improvement of V1, allowing to segment the TUG in three sub-phases: Sit-Stand, walking, Stand-Sit. These algorithms have been declined in a variant with the five sensors mentioned, and one without the sensor of the left femur.
The performance of the algorithms was compared to manual labeling performed on video. The comparison includes a bland-Altman plot and a correlation for the total test duration, but also for the sub-phase’s duration according to the two variants.
The TUG duration shows very good results regarding the limits of agreements (lLoA = -0.33 s and uLoA+0.6 s). The bias of 0.13 s indicated that the algorithm overrates the duration of the TUG. The results of the TUG subphases are less accurate. Although the correlation coefficient is between 0.76 and 0.96 for the different subphases, the limits of agreements are still very high, between -0.71 s and -0.5 s for the lLoA and +0.39 s and +0.58 s for the uLoA. These limits of agreements indicated that the Sit-Stand and Stand-Sit transition are not accurate enough yet. The dispersion is high for a transition that could last between about one and six seconds. The two variants, with and without a sensor on the left femur, present similar results.
The Project "Schluckspecht" of the University of Offenburg consists of participating in the European marathon called "Shell Eco-Marathon"(SEM) which consists of designing and building from the beginning a vehicle with the greatest possible energy efficiency. The University of Offenburg has participated in this project since 1998.
The team that forms the Schluckspecht project is made up of around 30 students from the faculties of mechanical engineering, process engineering, electrical engineering, medical technology and computer science, as well as the degree in Audiovisual Communication. The team was founded in 1998 and since then students have been developing and building high efficiency vehicles to participate in the European marathon Shell Eco.
In this project, students can put into practice all the theoretical knowledge obtained during their studies. Also can be learned how to work interdisciplinarity as a team, a skill that for now, many companies or require or seek.
The following topics are discussed in the Schluckspecht project, which are also ideal for the work of students:
-Conception construction and production of high efficiency vehicles.
-Computational design and manufacture of lightweight components and sets.
-Development of lightweight components and sets from renewable raw materials.
-Construction and development of special test benches, for example: motor test bench.
-Implementation and optimization of control strategies for autonomous driving
-Mechanical and electrical integration of sensors for autonomous driving
-Ergonomic studies and optimization of the driver's cabin.
The objective of the project is to develop and manufacture research vehicles that make individual mobility as efficient as possible from an energy point of view. To achieve this, current and future issues of the industry are discussed. In this project, both the theoretical and practical part of the light construction of vehicles and the reduction of friction, the variety of propulsion concepts (electric thrusters, fuel cells, diesel/petrol engines, Stirling engines) and autonomous driving are investigated. The services of the University of Offenburg together with some external partners are grouped together to make this wonderful project work.
The Projekt-Sweaty is a project of the University of Applied Sciences of Offenburg, an autonomous robot is being developed that competes against a set of several international colleges and universities in the RoboCup.
"Sweaty" is a soccer-playing humanoid robot who participated in the RoboCup World Cup in Brazil for the first time in 2014.
RoboCup is a competition aimed at developing a robot soccer team that surpasses the human world champion team. The competition started in 1997 the first official RoboCup games and conferences were held with great success. More than 40 teams took part and more than 5,000 spectators attended. RoboCup’s rules change to promote advances in robot science and technology and to bring the league’s challenges closer to the real world.
Building a robot that plays football will not in itself generate a significant social and economic impact, but the realization will certainly be considered an important success for the field of robotics.
Thanks to the interaction of all the faculties, the team consists of professors and students from the fields of mechanical and process engineering, electrical engineering, information technology, and information and media technology. Students can use the project during their studies and use the knowledge acquired in practice to implement and through their own creative ideas complement.
Decarbonisation Strategies in Energy Systems Modelling: APV and e-tractors as Flexibility Assets
(2023)
This work presents an analysis of the impact of introducing Agrophotovoltaic technologies and electric tractors into Germany’s energy system. Agrophotovoltaics involves installing photovoltaic systems in agricultural areas, allowing for dual usage of the land for both energy generation and food production. Electric tractors, which are agricultural machinery powered by electric motors, can also function as energy storage units, providing flexibility to the grid. The analysis includes a sensitivity study to understand how the availability of agricultural land influences Agrophotovoltaic investments, followed by the examination of various scenarios that involve converting diesel tractors to electric tractors. These scenarios are based on the current CO2 emission reduction targets set by the German Government, aiming for a 65% reduction below 1990 levels by 2030 and achieving zero emissions by 2045. The results indicate that approximately 3% of available agricultural land is necessary to establish a viable energy mix in Germany. Furthermore, the expansion of electric tractors tends to reduce the overall system costs and enhances the energy-cost-efficiency of Agrophotovoltaic investments.
Quarz crystal microbalances allow the monitoring of the adsorption process of mass from a liquid to their surface. The adsorbed mass can be analysed regarding to its protein content using mass spectromety. To ensure the protein identification the results of several measurements can be combined. A high content QCM-D array was developed to allow up to ten measurements parallel. The samples can be routed inside the array distributing one sample to several chips. The fluidic parts were prototyped using 3D printing. The assembled array was tight and the sample routing function could be demonstrated. A temperature controller was developed and implemented. The parameters for the PID controller were determined and the controller was shown to be able to keep the temperature constant over long time with high accuracy.
The purpose of this master's thesis was to set up a test bed for the absorption of chemical compounds by carbon-based sorbents and polymers and to develop a method for the detection of these substances applied by liquid chromatography.
The study made it possible to demonstrate the effectiveness of both polymers and biochars sorbents for the adosorption of specific substances. The results obtained open new paths on the study of biochar for the treatment of contaminated water. Some biochars made from plant-based materials have been shown to be almost as effective as commercial products used in plants. The developed chromatography method allows efficient separation of substances and their detection.
The interest of scientists to study motion sequences exists in the fields of sports science, clinical analysis and computer animation for quite some time. While in the last decades mainly markerbased motion capture systems have been used to evaluate movements, the interest in markerless systems is growing more and more. Nevertheless, in the field of clinical analysis, markerless methods have not yet proven their value, partly due to a lack of studies evaluating the quality of the obtained data. Therefore, this study aims to validate two markerless motion capture softwares from Simi Reality Motion Systems. The software Simi Shape, which is a mixture of traditional image-based tracking supported by an artificial intelligence net (AI net), and the software Crush, that uses a completely AI-based method. For this purpose, all motion data was recorded with two in-house motion capture systems. One system for recording the movements for a markerbased evaluation as gold standard and one system for markerless tracking. Within a laboratory environment, eight cameras per system were mounted around the area of motion. By placing two cameras in the same position and using the same calibration, deviations in the image data between those for markerbased and markerless tracking were extremely minimal. Based on this data, markerbased tracking was performed using the Simi Motion program, markerless tracking was performed using the Simi Shape software system and the latest software from Simi Reality Motion Systems, Crush. When comparing the markerless data with the markerbased data, an average root mean square error of 0,038 m was calculated for Simi Shape and a deviation of 0,037 m for Crush. In a direct comparison of the two markerless systems, a root mean square error of 0,019 m was scored. Based on these data, conclusions could be drawn about the accuracies of the two markerless systems. The obtained kinematic data of the tracking are in the range of high accuracy, which is limited to a deviation of less than 0,05 m according to the literature.
Estimation and projecting total steel industry production costs from 2019 to 2030 for Germany
(2023)
This thesis analyses the total production cost of the German steel industry from 2019 to 2022, as well as a projection of the German steel industry's total production cost until 2030. The research separates the costs of steel production into their primary components, such as raw materials, energy, CO2 cost, capital expenses and operating expenses. The cost of steel production is determined separately for primary steelmaking with the blast furnace and basic oxygen furnace (BF-BOF) and secondary steelmaking with the electric arc furnace (EAF).
The analysis indicates that, following the COVID-19 disaster and the fuel crisis, the overall cost of producing steel in Germany has progressively risen over the previous few years, reaching its peak in the first half of 2022. In addition, there are considerable disparities between the production costs of primary and secondary steelmaking processes, with primary steelmaking generally being more expensive.
In this analysis, the total cost of production for the German steel industry in the year 2030 has been estimated by taking into account historical trends as well as other predictions that are currently available.
This thesis provides overall insights on the economics of the German steel sector. By giving thorough information on production costs and changes over time, this research can assist guide crucial future investment decisions in this essential industry. To ensure long-term success, our findings emphasize the significance of investing in more sustainable and ecologically friendly steel production processes.