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Previous studies of the hyphenation of gas chromatographic separation and spectrophotometric detection in the ultraviolet wavelength range between 168 and 330 nm showed a high potential for applications where the analysis of complex samples is required. Within this paper the development of a state-of-the-art detection system for compounds in the vapour phase is described, offering an improved behaviour compared to previous systems: Dependent on the requirements of established detection systems hyphenated with gas chromatography, the main components of the system have to be designed for optimum performance and reliability of the spectrophotometric detector: A deuterium lamp as a broadband light source has been selected for improved stability in the measurements. A new-type absorption cell based on fiber-optics has been developed considering the dynamic necessary to compete with existing techniques. In addition, the influence of the volume of the cell on the chromatogram needs to be analyzed. Tests for determining the performance of the absorption cell in terms of chemical and thermal influences have been carried out. A new spectrophotometer with adequate spectral resolution in the wavelength range, offering improved stability and dynamic for an efficient use in this application was developed. Furthermore, the influence of each component on the performance, reliability and stability of the sensor system will be discussed. An overview and outlook over the potential applications in the environmental, scientific and medical field will be given.
In thin-layer chromatography, fiber-bundle arrays have been introduced for spectral absorption measurements in the UV-region. Using all-silica fiber bundles, the exciting light will be detected after re-emission on the plate with a fiberoptic spectrometer. In addition, fluorescence light can be detected which will be masked by the re-emitted light. Therefore, it is helpful to separate the absorption and fluorescence on the TLC-plate. A modified three-array assembly has been developed: using one array for detection, the two others are used for excitation with broadband band deuterium-light and with UV-LEDs adjusted to the substances under test. As an example, the quantification of glucosamine in nutritional supplements or spinach leaf extract will be described. Using simply heating of the amino-plate for derivation, the reaction product of Glucosamine can be detected sensitively either by light absorption or by fluorescence, using the new fiber-optic assembly. In addition, the properties of the new 3-row fiber-optic array and the commercially available UV-LEDs will be shown, in the interesting wavelength region for excitation of fluorescence, from 260 nm to 360 nm. The squint angle having an influence on coupling efficiency and spatial resolution will be measured with the inverse farfield method. Some properties of UV-LEDs for analytical applications will be described and discussed, too.
Polyarticulated active prostheses constitute a promising solution for upper limb amputees. The bottleneck for their adoption though, is the lack of intuitive control. In this context, machine learning algorithms based on pattern recognition from electromyographic (EMG) signals represent a great opportunity for naturally operating prosthetic devices, but their performance is strongly affected by the selection of input features. In this study, we investigated different combinations of 13 EMG-derived features obtained from EMG signals of healthy individuals performing upper limb movements and tested their performance for movement classification using an Artificial Neural Network. We found that input data (i.e., the set of input features) can be reduced by more than 50% without any loss in accuracy, while diminishing the computing time required to train the classifier. Our results indicate that input features must be properly selected in order to optimize prosthetic control.
A smart energy concept was designed and implemented for a cluster of 5 existing multi-family houses, which combines heat pumps, photovoltaic (PV) modules and combined heat and power units (CHP) to achieve energy- and cost-efficient operation. Measurement results of the first year of operation show that the local power generation by PV modules and CHP unit has a positive effect on the electrical self-sufficiency by reducing electricity import from the grid. In winter, when the CHP unit operates continuously for long periods, the entire electricity for the heat pump and 91 % of the total electricity demand of the neighborhood are supplied locally. In summer, only 53 % is generated within the neighborhood. The use of a specifically developed energy management system EMS is intended to further increase this share. CO2 emissions for heating and electricity of the neighborhood are evaluated and amount to 18.4 kg/(m2a). Compared to the previous energy system consisting of gas boilers (29.1 kg/(m2a)), savings of 37 % are achieved with electricity consumption from the grid being reduced by 65 %. In the second construction stage, an additional heat pump, CHP unit and PV modules will be added. The measurement results indicate that the final district energy system is likely to achieve the ambitious CO2 reduction goal of -50% and further increase the self-sufficiency of the district.
Eco-innovations in chemical processes should be designed to use raw materials, energy and water as efficiently and economically as possible to avoid the generation of hazardous waste and to conserve raw material reserves. Applying inventive principles identified in natural systems to chemical process design can help avoid secondary problems. However, the selection of nature-inspired principles to improve technological or environmental problems is very time-consuming. In addition, it is necessary to match the strongest principles with the problems to be solved. Therefore, the research paper proposes a classification and assignment of nature-inspired inventive principles to eco-parameters, eco-engineering contradictions and eco-innovation domains, taking into account environmental, technological and economic requirements. This classification will help to identify suitable principles quickly and also to realize rapid innovation. In addition, to validate the proposed classification approach, the study is illustrated with the application of nature-inspired invention principles for the development of a sustainable process design for the extraction of high-purity silicon dioxide from pyrophyllite ores. Finally, the paper defines a future research agenda in the field of nature-inspired eco-engineering in the context of AI-assisted invention and innovation.
Encapsulant-free N.I.C.E. modules have strong ecological advantages compared to conventional laminated modules but suffer generally from lower electrical performance. Via long-term outdoor monitoring of fullsize industrial modules of both types with identical solar cells, we investigated if the performance difference remains constant over time and which parameters influence its value. After assessing about a full year’s data, two obvious levers for N.I.C.E. optimization are identified: The usage of textured glass and transparent adhesives on the module rear side. Also, the performance loss could be alleviated using tracking systems due to lower AOI values. Our measurements show additionally that N.I.C.E. module surfaces are in average about 2.5°C cooler compared to laminated modules. With these findings, we lay out a roadmap to reduce today’s LIV gap of about 5%rel by different optimizations.
In this paper, we propose an approach for gait phase detection for flat and inclined surfaces that can be used for an ankle-foot orthosis and the humanoid robot Sweaty. To cover different use cases, we use a rule-based algorithm. This offers the required flexibility and real-time capability. The inputs of the algorithm are inertial measurement unit and ankle joint angle signals. We show that the gait phases with the orthosis worn by a human participant and with Sweaty are reliably recognized by the algorithm under the condition of adapted transition conditions. E.g., the specificity for human gait on flat surfaces is 92 %. For the robot Sweaty, 95 % results in fully recognized gait cycles. Furthermore, the algorithm also allows the determination of the inclination angle of the ramp. The sensors of the orthosis provide 6.9 and that of the robot Sweaty 7.7 when walking onto the reference ramp with slope angle 7.9.
Selbsttests in Lernmanagementsystemen (LMS) ermöglichen es Studierenden, den eigenen Lernfortschritt einzuschätzen. Im Gegensatz zur Einreichung und Korrektur vollständig ausformulierter Aufgabenlösungen nutzen LMS überwiegend die Eingabe der Lösung im Antwort-Auswahl-Verfahren (Single-Choice). Nach didaktischen Ansatz „Physik durch Informatik“ geben die Lernenden stattdessen ihre Aufgabenlösungen in einer Programmiersprache ins LMS ein, was eine automatisierte Rückmeldung erleichtert und das Erreichen einer höheren Kompetenzstufe fördert. Es wurden zehn LMS-Selbsttests erstellt, bei denen die Lösungen zu einer Lehrbuch-Aufgabenstellung jeweils durch Eingabe in einer Programmiersprache und von einer Kontrollgruppe im Antwort-Auswahl-Verfahren abgefragt wurden. Ergebnisse aus dem ersten Einsatz dieser Selbsttests für die Lehrveranstaltung Physik im Studiengang Biotechnologie werden vorgestellt.
In this paper we report on further success of our work to develop a multi-method energy optimization which works with a digital twin concept. The twin concept serves to replicate production processes of different kinds of production companies, including complex energy systems and test market interactions to then use them for model predictive optimizing. The presented work finally reports about the performed flexibility assessment leading to a flexibility audit with a list of measures and the impact of energy optimizations made related to interactions with the local power grid i.e., the exchange node of the low voltage distribution grid. The analysis and continuous exploration of flexibilities as well as the exchange with energy markets require a “guide” leading to continuous optimization with a further tool like the Flexibility Survey and Control Panel helping decision-making processes on the day-ahead horizon for real production plants or the investment planning to improve machinery, staff schedules and production
infrastructure.
Turbocharger housings in internal combustion engines are subjected to severe mechanical and thermal cyclic loads throughout their life-time or during engine testing. The combination of thermal transients and mechanical load cycling results in a complex evolution of damage, leading to thermo-mechanical fatigue (TMF) of the material. For the computational TMF life assessment of high temperature components, the DTMF model can provide reliable TMF life predictions. The model is based on a short fatigue crack growth law and uses local finite-element (FE) results to predict the number of cycles to failure for a technical crack. In engine applications, it is nowadays often acceptable to have short cracks as long as they do not propagate and cause loss of function of the component. Thus, it is necessary to predict not only potential crack locations and the corresponding number of cycles for a technical crack, but also to determine subsequent crack growth or even a possible crack arrest. In this work, a method is proposed that allows the simulation of TMF crack growth in high temperature components using FE simulations and non-linear fracture mechanics (NLFM).
A NLFM based crack growth simulation method is described. This method starts with the FE analysis of a component. In this paper, the method is demonstrated for an automotive turbocharger housing subjected to TMF loading. A transient elastic-viscoplastic FE analysis is used to simulate four heating and cooling cycles of an engine test. The stresses, inelastic strains, and temperature histories from the FEA are then used to perform TMF life predictions using the standard DTMF model. The crack position and the crack plane of critical hotspots are then identified. Simulated cracks are inserted at the hotspots. For the model demonstrated, cracks were inserted at two hotspot locations. The ΔJ integral is computed as a fracture mechanics parameter at each point along the crack-front, and the crack extension of each point is then evaluated, allowing the crack to grow iteratively. The paper concludes with a comparison of the crack growth curves for both hotspots with experimental results.