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We report the use of the Raman spectral information of the chemical compound toluene C7H8 as a reference on the analysis of laboratory-prepared and commercially acquired gasoline-ethanol blends. The rate behavior of the characteristic Raman lines of toluene and gasoline has enabled the approximated quantification of this additive in commercial gasoline-ethanol mixtures. This rate behavior has been obtained from the Raman spectra of gasoline-ethanol blends with different proportions of toluene.
All these Raman spectra have been collected by using a self-designed, frequency precise and low-cost Fourier-transform Raman spectrometer (FT-Raman spectrometer) prototype. This FT-Raman prototype has helped to accurately confirm the frequency position of the main characteristic Raman lines of toluene present on the different gasoline-ethanol samples analyzed at smaller proportions than those commonly found in commercial gasoline-ethanol blends. The frequency accuracy validation has been performed by analyzing the same set of toluene samples with two additional state-of-the-art commercial FT-Raman devices. Additionally, the spectral information has been contrasted, with highly-correlated coefficients as a result, with the values of the standard Raman spectrum of toluene.
La industria del bacanora en Sonora, México, enfrenta la influencia de una compleja red de factores culturales, tecnológicos, económicos y legales que inhiben su desarrollo. Ello ocurre pese al esfuerzo institucional por radicar un marco normativo que elimine la práctica de los métodos informales de elaboración que derivan en calidades heterogéneas de licor. El conseguirlo se complica ante la dificultad que enfrentan los actores de esta industria para implementar prácticas efectivas de verificación de las normas vigentes en los confines de la geografía de la Denominación de Origen. En este documento se describe el uso de un prototipo de espectrómetro Raman por transformada de Fourier para analizar cualitativamente muestras desconocidas de bacanora. Este dispositivo se construyó con el uso de un interferómetro Michelson convencional, un contador de fotones de diseño propio y un foto-detector de referencia. Los resultados del trabajo confirman que dada su naturaleza de diseño y construcción, este instrumento de medición y su efectiva técnica de operación a bajo costo, constituye una alternativa viable, adaptable fácilmente a las necesidades de los actores productivos e institucionales, para asistirlos en la elaboración de bacanora y a la verificación de su calidad conforme a los criterios de la normatividad.
The Raman spectra from the chemical compounds toluene and cyclohexane obtained using a Fourier Transform (FT)-Raman spectrometer prototype have been contrasted with the Raman spectra of these same materials collected with two different commercial FT-Raman devices. The FT-Raman spectrometer consist of a Michelson interferometer, a self-designed photon counter and a reference photo-detector. The evaluation methodology of the spectral information, contrary to the commercial devices that commonly use the zero-crossing method, is carried out by re-sampling the Raman scattering and by accurately extracting the optical path information of the Michelson interferometer. The FTRaman arrangement has been built using conventional parts without disregarding the spectral frequency precision that usually such a FTRaman instruments deliver. No additional complex hardware components or costly software modules have been included in this FT-Raman device. The main Raman lines from the spectra obtained with the three FT-Raman devices have been compared with the Raman lines from the standard Raman spectra of these two materials. The values obtained using the FT-Raman spectrometer prototype have shown a frequency accuracy comparable to that obtained with the commercial devices without facing the need for a large investment. Although the proposed FT-Raman prototype cannot be directly compared to the last generation of FT-Raman spectrometers from the commercial manufacturers, such a device could give an opportunity to users that require high frequency precision in their spectral analysis and are provided with rather scarce resources.
Verfahren zur Bestimmung von Eigenschaften einer Rohrleitung, insbesondere der Position eines Abzweigs einer Abwasserrohrleitung,(a) bei dem ein Schallwellensendesignal (S, S') an einem vorgegebenen Einspeisepunkt in die Rohrleitung (1) eingespeist wird und sich in axialer Richtung der Rohrleitung (1) ausbreitet,(b) wobei das Frequenzspektrum des Schallwellensendesignals (S, S') eine Frequenzkomponente oder einen Spektralbereich aufweist, dessen maximale Frequenz kleiner ist als die untere Grenzfrequenz (f) für die erste Obermode,(c) bei dem innerhalb der Rohrleitung (1) reflektierte Anteile (S, S, S, S', S', S') des Schallwellensendesignals (S, S') als Schallwellenempfangssignal (E, E') detektiert werden, und(d) bei dem die Rohrleitung (1) durch eine Auswertung des Schallwellenempfangssignal (E, E') in Bezug auf das Schallwellensendesignal (S, S') hinsichtlich des Vorhandenseins von Schallwellenreflexionen (S, S, S, S', S', S') verursachenden Reflexionsorten entlang der Rohrleitung (1) untersucht wird,(e) wobei mittels der Auswertung des Schallwellenempfangssignals (E, E') zumindest jeweils der Abstand (I) eines Reflexionsortes von dem Einspeisepunkt bestimmt wird, dadurch gekennzeichnet,(f) dass die Schallgeschwindigkeit (c) der Grundmode bei der aktuellen Temperatur innerhalb der Rohrleitung (1) unter Verwendung eines Schallwellenmesssignals ermittelt wird, welches eine Frequenz oder ein Frequenzspektrum aufweist, bei dem das Schallwellenmesssignal innerhalb der Rohrleitung (1) mit ausreichender Genauigkeit als ebene Schallwelle behandelt werden kann, wobei hierzu die Laufzeiten des Schallwellenmesssignals über eine vorbekannte Strecke (L) in beiden Richtungen gemessen wird,(g) dass die so ermittelte Schallgeschwindigkeit (c) einer ebenen Schallwelle gleich der tatsächlichen Schallgeschwindigkeit der Grundmode bei der aktuellen Temperatur innerhalb der Rohrleitung (1) gesetzt wird, und(h) dass die so bestimmte Schallgeschwindigkeit zur Bestimmung des Abstand (I) eines Reflexionsortes von dem Einspeisepunkt verwendet wird.
Vorrichtung und Verfahren zur optischen Messung der Entfernung eines Objekts (DE102007060966A1)
(2009)
Eine Vorrichtung zur optischen Messung der Entfernung eines Objekts weist eine Quelle zur Aussendung optischer Strahlung, die eine eine optische Strahlung transportierende Lichtleitfaser aufweist, ein optisches Element, welches die optische Strahlung fokussiert und auf das Objekt abbildet, und einen Empfänger auf, der die optische Strahlung empfängt und in ein elektrisches Signal zur Weitergabe an eine Steuereinrichtung umwandelt. Die Lichtleitfaser ist mittels einer Verschiebeeinrichtung relativ zu dem optischen Element verschieblich. Ein Abschnitt der Lichtleitfaser führt zu dem Empfänger und ist mittels einer Kopplungseinrichtung mit einem von der Quelle zur Aussendung optischer Strahlung ausgehenden Abschnitt der Lichtleitfaser zu einer einzigen, mittels der Verschiebeeinrichtung verschieblichen Lichtleitfaser gekoppelt.
The device (1) has a detection unit (38) that is provided for detecting two electromagnetic radiations that are radiated by a light source (10) after partial radiography of a medium with applied magnetic field (44). A determination unit (40) is provided for determining a phase relation between the two detected electromagnetic radiations. An evaluation unit (46) is provided for determining a concentration value of a magneto-optic substance in the medium on the basis of the determined phase relation. Independent claims are also included for the following: (1) a method for determining concentration value of a magneto-optic substance in a medium (2) a computer program product for performing a method for determining concentration value of a magneto-optic substance in a medium.
A method for determining properties of a pipeline includes feeding a sound wave signal at a predetermined feed point into the pipeline so that the sound wave signal propagates in an axial direction of the pipeline. The frequency spectrum of the transmitted sound wave signal has a frequency component or a spectral range with a maximum frequency that is smaller than the lower limit frequency for the first upper mode. Reflected portions of the transmitted sound wave signal are detected as received sound wave signal and are evaluated with regard to the transmitted sound wave signal to determine at least the distance of each reflection site from the feed point.
The fast and cost-effective manufacturing of tools for thermoforming is an essential requirement to shorten the development time of products. Thus, additive processes are used increasingly in tooling for thermoforming of plastic sheets. However, a disadvantage of many additive methods is that they are highly cost-intensive, since complex systems based on laser technology and expensive metal powders are needed. Therefore, this paper examines how to work with favorable additive methods, e.g. Binder Jetting, to manufacture tools, which provide sufficient strength for thermoforming. The use of comparatively low-priced inkjet technology for the layer construction and a polymer plaster as material can be expected to result in significant cost reductions. Based on a case study using a cowling (engine bonnet) for an Unmanned Aerial Vehicle (UAV), the development of a complex tool for thermoforming is demonstrated. The object in this study is to produce a tool for a complex-shaped component in small numbers and high quality in a short time and at reasonable costs. Within the tooling process, integrated vacuum channels are implemented in additive tooling without the need for additional post-processing (for example, drilling). In addition, special technical challenges, such as the demolding of undercuts or the parting of the tool are explained. All process steps from tool design to the use of the additively manufactured tool are analyzed. Based on the manufacturing of a small series of cowlings for a UAV made of plastic sheets (ABS), it is shown, that the Binder Jetting offers sufficient mechanical and thermal strength for additive tooling. In addition, an economic evaluation of the tool manufacturing and a detailed consideration of the required manufacturing times for the different process steps are carried out. Finally, a comparison is made with conventional and alternative additive methods of tooling.